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The analysis of volatile flavor components of Jin Xiang garlic and Tai’an garlic

机译:金香大蒜和泰安大蒜的挥发性风味成分分析

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The volatile flavor compounds of Jin Xiang garlic and Tai’an garlic in chemical composition were detected and analyzed and the contents of them were compared and determinated. The volatile constituents of Jin Xiang garlic and Tai’an garlic were compared and analyzed by automatic static headspace and gas chromatography-mass spectrometry. Qualitative analysis of samples was made through the analysis of gas chromatography-mass spectrometry and NIST mass spectral library computer retrieval, and quantitative analysis was made by using area normalization method. The analysis results show that the slight difference of the volatile flavor compounds was detected in different places of origin garlic and Jin Xiang garlic was detected more total sulfur-containing compounds than Tai’an garlic. Meanwhile, the contents of sulfur compounds of the fresh garlic were more than the stored garlic and there were significant differences between them. The tests results indicated that flavor substances’ types were slightly different between Jin Xiang garlic and Tai’an garlic, and regional differences cannot affect the garlic flavor substances type. Jin Xiang garlic has more obvious flavor substances than Tai’an garlic which play a decisive role in the garlic flavor, such as 1,3-dithiane, and allyl trisulfide and allyl disulfide and diallyl tetrasulphide. The result of this research indicates that Automatic static headspace and gas chromatography-mass spectrometry is a fast, easy, efficient and accurate method to analyze and identify the volatile flavor components of garlic.
机译:对金香大蒜和泰安大蒜的挥发性风味物质的化学成分进行了检测和分析,并对其含量进行了比较和测定。通过自动静态顶空和气相色谱-质谱法对金香大蒜和泰安大蒜的挥发性成分进行了比较和分析。通过气相色谱-质谱分析和NIST质谱库计算机检索对样品进行定性分析,并使用面积归一化方法进行定量分析。分析结果表明,在不同产地的大蒜中检测到挥发性风味化合物的细微差异,在金香大蒜中检测到的总含硫化合物比泰安大蒜更多。同时,鲜蒜中的硫化合物含量高于贮藏的大蒜,两者之间存在显着差异。测试结果表明,金香大蒜和泰安大蒜的风味物质类型略有不同,区域差异不会影响大蒜风味物质的类型。金香大蒜比泰安大蒜具有更明显的风味物质,它们对大蒜的风味起决定性作用,例如1,3-二噻吩,烯丙基三硫化物,烯丙基二硫化物和二烯丙基四硫化物。研究结果表明,自动静态顶空和气相色谱-质谱联用法是一种快速,简便,高效,准确的分析和鉴定大蒜中挥发性风味成分的方法。

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