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Effect of aluminum silicate fiber modification on crack-resistance of a ceramic mould

机译:硅酸铝纤维改性对陶瓷模具抗裂性能的影响

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To improve the crack-resistance of the mould for silica sol bonded quartz based ceramic mould casting, aluminum silicate fibers with the diameter ranging from 5 μm to 25 μm and the length about 1 mm were dispersed in the ceramic mould. The effect of the aluminum silicate fibers on the tensile strength, shrinkage rate and the cracking trend of the ceramic mould were investigated. In the ceramic slurry, quartz sand was applied as ceramic aggregate, silica sol containing 30% silicon dioxide as bonder, and the weight ratio of quartz sand to silica sol was 2.69; the dispersed fibers changed from 0 to 0.24vol.%. The mould samples were formed after the slurry was poured and gelled at room temperature, and then sintered at different temperatures ranging from 100 to 800 ℃ to measure the tensile strength and shrinkage rate. The results show that, with the aluminum silicate fiber addition increasing from 0 to 0.24vol.%, the tensile strength increases linearly from 0.175 MPa to 0.236 MPa, and the shrinkage rate decreases linearly from 1.75% to 1.68% for the ceramic mould sintered at 400 ℃, from 1.37% to 1.31% for the ceramic mould at room temperature. As the sintering temperature was raised from 100 ℃ to 800 ℃, the tensile strength increases, and the shrinkage rate decreases at all temperatures, compared with those without fiber dispersion, but their variation patterns remain the same. Furthermore, the cracking trend of the mould and its decreasing proportion were defined and analyzed quantitatively considering both effects of the fiber dispersion on the strength and shrinkage. The cracking trend appears to decrease linearly with increasing fiber content and to reach the maximum reduction of 28.8% when 0.24vol.% fiber was dispersed. Therefore, the investigation proposes a new method to improve the crack-resistance of the ceramic mould, i.e., inorganic fiber dispersion into the ceramic mould.
机译:为了提高用于二氧化硅溶胶结合的石英基陶瓷铸模的模具的抗裂性,将直径为5μm至25μm且长度为约1mm的硅酸铝纤维分散在陶瓷模具中。研究了硅酸铝纤维对陶瓷模具拉伸强度,收缩率和开裂趋势的影响。在该陶瓷浆料中,以石英砂作为陶瓷骨料,以含有30%二氧化硅的硅溶胶作为粘结剂,石英砂与硅溶胶的重量比为2.69。分散的纤维从0变为0.24vol。%。在室温下将浆料倒入并凝胶化后,形成模具样品,然后在100至800℃的不同温度下烧结,以测量拉伸强度和收缩率。结果表明,随着添加量的增加,硅酸铝纤维的添加量从0增加到0.24vol。%,拉伸强度从0.175 MPa线性增加到0.236 MPa,收缩率从1.75%线性减少到1.68%。 400℃时,从1.37%到1.31%为陶瓷模具在室温下。与没有纤维分散的情况相比,当烧结温度从100℃提高到800℃时,在所有温度下的抗拉强度均增加,收缩率降低,但其变化规律保持不变。此外,考虑到纤维分散对强度和收缩率的影响,定义并定量分析了模具的开裂趋势及其减少的比例。随着纤维含量的增加,开裂趋势似乎呈线性下降,而当分散0.24vol。%的纤维时,开裂趋势达到最大的下降28.8%。因此,研究提出了一种新的方法来改善陶瓷模具的抗裂性,即无机纤维分散到陶瓷模具中。

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