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Laser shock peening without coating induced residual stress distribution, wettability characteristics and enhanced pitting corrosion resistance of austenitic stainless steel

机译:没有涂层的激光冲击喷丸会引起残余应力分布,润湿性和增强的奥氏体不锈钢抗点蚀性能

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Low energy laser shock peening without coating (LSPwC) was conducted on AISI 304 austenitic stainless steel specimens with varying pulse densities or overlapping. Highest magnitude of compressive residual stress (CRS) was achieved for an optimized pulse density of 2500 pulses/cm(2) (75% overlapping). The 2-D and 3-D topographical analysis were indicative of the fact that controlled roughening of the surface was achieved after the LSPwC process. After the LSPwC process, the hydrophilic unpeened surface was converted into the hydrophobic surface, thus decreasing the wettability characteristics of the surface. The X-ray diffraction (XRD) results reveal that there is a beginning of the martensite transformation and the rise in the intensity value of the peaks after LSPwC indicates the presence of compressive residual stresses induced in the specimen. The optical microscope and high-resolution transmission electron microscope results provided evidence of grain refinement and deformation induced refinement features such as multidirectional mechanical twinning, dislocations lines, micro shear cells and stacking faults in the near and sub-surface areas. The average hardness value of the LSPwC specimens was found to be increased by 28% more than the untreated specimen. The potentiodynamic polarization revealed that there was a considerable amount of increase in the pitting corrosion resistance after the LSPwC process, thus, supporting to extend the fatigue life of the specimen. The electrochemical impedance spectroscopic (EIS) analysis depicts that the LSPwC process supports the formation of the strong passivation layer in 3.5% NaCl solution. (C) 2017 Elsevier B.V. All rights reserved.
机译:对AISI 304奥氏体不锈钢试样进行了低能激光无涂层冲击喷涂(LSPwC),该试样具有不同的脉冲密度或重叠。对于2500脉冲/ cm(2)(75%重叠)的优化脉冲密度,可以达到最高的压缩残余应力(CRS)强度。 2-D和3-D形貌分析表明,在LSPwC处理后,表面可控粗糙化。经过LSPwC处理后,亲水性未喷丸表面转化为疏水性表面,从而降低了表面的润湿性。 X射线衍射(XRD)结果表明存在马氏体转变的开始,并且在LSPwC指示样品中存在压缩残余应力后,峰强度值的升高。光学显微镜和高分辨率透射电子显微镜的结果提供了晶粒细化和变形诱导的细化特征的证据,例如多方向机械孪晶,位错线,微剪切单元和近表层和下表层区域的堆积断层。发现LSPwC样品的平均硬度值比未处理的样品增加了28%。电位动力学极化表明,在LSPwC处理后,抗点蚀性能有了相当大的提高,从而有助于延长样品的疲劳寿命。电化学阻抗谱(EIS)分析表明LSPwC工艺支持在3.5%NaCl溶液中形成强钝化层。 (C)2017 Elsevier B.V.保留所有权利。

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