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Optimized ultrasonic‐assisted extraction of papaya seed oil from Hainan/Eksotika variety

机译:超声波辅助从海南/依索提卡品种中提取木瓜籽油的优化工艺

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摘要

Hainan/Eksotika papaya is a popular cultivated plant in Hainan Island, China. Papaya seed oil (PSO) contains functional compounds with good antioxidant activity, especially monounsaturated fatty acids. In this work, the ultrasound‐assisted extraction (UAE) of PSO was optimized using response surface methodology. It was found that the optimal extraction performance was realized when the elevated time was set to 20 min, the ultrasound power was set to 250 W, and the n‐hexane‐to‐sample ratio was set to 16:1 (v/w). The highest yield of PSO (32.27%) was obtained under the optimal conditions, and PSO showed good oxidative stability. Differential scanning calorimetry analysis showed that the melting point of Hainan/Eksotika PSO was low, while its crystallization temperature was high. FTIR and NMR were used to analyze the chemical structure of PSO, which also proved that PSO possessed good stability without oxidative degradation. In addition, scanning electron micrograph was employed to investigate the change in seed microscopic structure. The results showed UAE caused serious structural damage of sample cell membranes and walls, which help oil access to the solvent with a high extraction ratio. The results indicated that UAE is an efficient environmental‐friendly, and promising technique could be applied to produce PSO or other edible oil with a better health‐beneficial value in food industry.
机译:Hainan / Eksotika木瓜是中国海南岛的一种流行栽培植物。木瓜籽油(PSO)包含具有良好抗氧化活性的功能化合物,尤其是单不饱和脂肪酸。在这项工作中,使用响应面方法优化了PSO的超声辅助提取(UAE)。发现将延长时间设置为20分钟,将超声功率设置为250 W,将正己烷与样品的比例设置为16:1(v / w)可以实现最佳的提取性能。在最佳条件下获得了最高的PSO收率(32.27%),并且PSO具有良好的氧化稳定性。差示扫描量热法分析表明,海南/埃索托卡PSO的熔点较低,而结晶温度较高。用FTIR和NMR分析了PSO的化学结构,也证明了PSO具有良好的稳定性而不会发生氧化降解。另外,采用扫描电子显微镜观察种子的微观结构变化。结果表明,阿联酋对样品细胞膜和壁造成了严重的结构破坏,这有助于油以较高的萃取率进入溶剂。结果表明,阿联酋是一种高效的环境友好型技术,可以应用于生产食品工业中具有更好的健康有益价值的PSO或其他食用油。

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