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The role of breadfruit OSA starch and surfactant in stabilizing high-oil-load emulsions using high-pressure homogenization and low-frequency ultrasonication

机译:面包果OSA淀粉和表面活性剂在稳定高油负载乳液中使用高压均质化和低频超声的作用

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摘要

This study aimed to investigate the role of modified breadfruit starch in the presence of Tween 80 for stabilizing the oil-in-water emulsions. An ultra turrax homogenizer was used to produce coarse emulsions, followed by high-pressure homogenization (HPH) or low-frequency ultrasonication (LFU) for fine emulsions. The breadfruit starch was chemically modified using octenyl succinic anhydride (OSA) to produce modified breadfruit OSA starch (BOSA). The dispersed phase was a mixture of palm and lemon oil in a 9:1 ratio. Two BOSA (1% and 2%), three oil concentrations (10%, 25%, and 40%) and Tween 80 (1% of the total amount of oil) were examined based on the emulsion stability. The Fourier transform infrared spectroscopy (FTIR) indicated that starch modification was successful (Degree of Substitution-DS, 0.0241). The most stable coarse emulsions contained 40% oil and 2% BOSA starch. The same formula produced fine emulsions that remained stable for over 42 days, regardless of the homogenization method. BOSA starch and Tween 80 exhibit a mixed stabilization effect on the oil-in-water emulsions. HPH produced more uniformly sized emulsion droplets when compared with those produced using LFU.
机译:本研究旨在探讨改性的面包丁淀粉在吐温80中的作用,以稳定水包油乳液。超涡轮均化器用于产生粗乳液,然后进行高压均质化(HPH)或低频超声(LFU),用于细乳液。使用辛烯基琥珀酸酐(OSA)化学改性面包果淀粉以产生改性的面包果OSA淀粉(BOSA)。分散相是棕榈和柠檬油的混合物,在9:1的比例中。基于乳液稳定性,检查了两种乳腺素(1%和2%),三种油浓度(10%,25%和40%)和吐温80(占油的总量的1%)。傅里叶变换红外光谱(FTIR)表明淀粉改性成功(取代度-DS,0.0241)。最稳定的粗乳液含有40%的油和2%Bosa淀粉。与均质化方法无关,相同的配方生产的细乳液持续超过42天。 BOSA淀粉和吐温80对水包油乳液表现出混合稳定效果。与使用LFU产生的那些相比,HPH产生更均匀大小的乳液液滴。

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