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Grafting C8-C16 alkyl groups altered the self-assembly and curcumin –loading properties of sodium caseinate in water

机译:C8-C16烷基的接枝改变了酪蛋白酸钠在水中的自组装和姜黄素负载特性

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摘要

The data presented here are related to the research article entitled “Synthesis and characterization of alkylated caseinate, and its structure-curcumin loading property relationship in water” (Zhang et al., 2018) . This data article reports the detailed spectra information for 1H NMR, 13C NMR and UPLC-Q-TOF MS of the N-succinimidyl fatty acid esters with various alkyl chain lengths (Cn-NHSs, n = 8, 12, 14 and 16). 1H NMR, 13C NMR and UPLC-Q-TOF MS spectra for C16-NHS are shown as an example. Then the stacked 1H NMR spectra of the obtained alkylated caseinates (Cn-caseinates, n = 8, 12, 14 and 16) are provided. The surface hydrophobicity index (S0) of Cn-caseinates with different substitution degrees (SD) of alkyl groups is shown. Additionally, Visual appearances for the formed aqueous dispersions of curcumin-loaded native caseinate (NaCas) and Cn-caseinates self-assemblies are shown. X-ray diffraction patterns of curcumin, C16-caseinate, its physical mixture and curcumin-loaded C16-caseinate self-assemblies are examined. The re-dispersibility and short-term storage stability of the curcumin-loaded NaCas and C16-caseinate self-assemblies are also studied.
机译:此处提供的数据与题为“烷基化酪蛋白酸盐的合成与表征及其在水中的结构-姜黄素负载性质关系”的研究文章有关(Zhang等人,2018)。该数据文章报告了具有各种烷基链长的N-琥珀酰亚胺基脂肪酸酯的 1 H NMR, 13 C NMR和UPLC-Q-TOF MS的详细光谱信息(C n -NHS,n = 8、12、14和16)。以C16-NHS的 1 H NMR, 13 C NMR和UPLC-Q-TOF MS光谱为例。然后提供所获得的烷基化酪蛋白酸酯(Cn-酪蛋白酸酯,n = 8、12、14和16)的堆叠的 1 1 H NMR谱。显示了具有不同烷基取代度(SD)的Cn-酪蛋白酸盐的表面疏水性指数(S0)。此外,显示了姜黄素负载的天然酪蛋白酸盐(NaCas)和Cn-酪蛋白酸盐自组装物形成的水分散体的视觉外观。检查了姜黄素,C16酪蛋白酸盐,其物理混合物和负载姜黄素的C16酪蛋白酸盐自组装体的X射线衍射图。还研究了姜黄素负载的NaCas和C16-酪蛋白酸盐自组装体的可再分散性和短期储存稳定性。

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