在80%Al−20%CuO(质量分数)体系中，通过原位反应法制备Al2O3p−Al复合材料。采用不同方法研究CuO颗粒粒度对复合材料合成温度和显微组织的影响。结果表明，CuO颗粒粒度对Al−CuO体系的完全反应温度有显著影响：含有粒度小于6μm CuO颗粒样品的完全反应温度比含有粒度小于100μm CuO颗粒样品的完全反应温度低200°C。当反应温度低于某一临界值时，原位Al2O3颗粒和Al基体之间不能完全结合；当温度高于某一临界值时，原位Al2O3颗粒的形貌从棒状转变成近球形。这两个临界温度受CuO颗粒粒度的影响：含有粒度小于6μm CuO颗粒样品的临界温度比含有小于100μm CuO颗粒样品的临界温度低100°C。%Al2O3p−Al composites were synthesized using an in-situ reaction in the 80%Al−20%CuO (mass fraction) system. The effects of the CuO particle size on the synthesis temperature and microstructure of the composites were investigated by various methods. The results indicate that the CuO particle size has a significant effect on the temperature at which the complete reaction in the Al−CuO system occurs:the temperature is 200 °C lower in the Al−CuO system containing CuO particles with sizes less than 6μm than that containing CuO particles with sizes less than 100μm. The interfacial bonding between Al2O3 particles and Al is not complete when the temperature is below a critical value. The morphology of the Al2O3 particles varies from ribbon-like shape to near spherical shape when the temperature is above a critical value. These two critical temperatures are affected by the particle size of CuO, and the critical temperature of the sample containing CuO particles with sizes less than 6μm is 100 °C lower than that of the sample containing CuO particles with sizes less than 100μm.
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