氨基甲酸酯型脱氧胆酸分子裂缝的微波合成

摘要

A series of novel molecular clefts were synthesized in good yields using deoxycholic acid as spacer to bridge different aromatic amines via triphosgene under microwave irradiation. The structures were confirmed by 1H NMR, IR, MS and elemental analysis.%在微波辐射条件下,以脱氧胆酸为隔离基,通过三光气桥连各种芳香胺,以良好的产率合成了一系列新的分子裂缝,其结构经1H NMR,IR,MS和元素分析确证.