样品前处理技术在气相色谱分析中的应用进展

摘要

Gas chromatography (GC) is a widely used analytical technique in many fields.Sample preparation is very important in GC analysis due to its time consumed and deviations produced.In the present paper,the progress of some typical sample preparation techniques in gas chromatography,including purge and trap,solid phase extraction,solid phase microextraction,liquid phase microextraction,microwave assisted extraction,ultrasonic-assisted extraction,etc.,are reviewed.%气相色谱法是当前应用最广泛的分析技术之一.使用气相色谱对复杂基体进行分析时的样品前处理步骤往往繁琐耗时,易引起误差,已成为制约分析效率和准确度提升的关键环节.本文综述了2009-2013年几种主要的样品前处理技术,包括吹扫捕集、固相萃取、固相微萃取、液相微萃取技术以及微波辅助萃取、超声波辅助萃取等场辅助萃取技术在气相色谱分析中的应用研究进展.