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Heat-transfer Mechanism of Sample-probe in Variable-temperature Scanning Probe Microscope and Influence of Temperature on Tunneling Current

机译:可变温度扫描探针显微镜中样品探针的热传递机理及温度对隧道电流的影响

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The macroscopical breakage and nature change of material usually originate in nanometer scale, and the nature of some materials depends on temperature strongly. So it is extremely important for the research of heat transfer in micro-scale and nanometer technology to understand and control the influence of temperature on the nature of material, and developing advanced measuring technique can also improve our knowledge on theories involved in such problem. Due to the usage of variable-temperature sample stage, utilizable range of temperature is widely extended, and thus topography images of materials changing with temperature can be observed so that the thermal properties of materials can be studied further. Accordingly, the theoretical basis of heat-transfer and the influence of temperature on tunneling current owing to temperature variation should be presented. In the view of microscale heat-transfer, this paper describes the problem that heat current transfers from surface of sample to tip of probe through layer of air by means of Boltzmann theory, which can be expressed by the hyperbolic equation of heat conduction when the time is nearly equivalent to slack time and the scale is much larger than the characteristic scale of local thermodynamic equilibrium. The mode of heat-transfer on probe is also analyzed and the analytical solution is obtained in the paper. In addition, the influence of temperature increment of sample on tunneling current is discussed in detail and the change trend of tunneling current with temperature is also obtained in a limited temperature range. Due to such factors, which are possible to disturb the topography images of sample, there is no doubt that many difficulties will be brought to developing new technology such as detecting displacement and strain of materials at microscale by using the images of sample heated and unheated. To understand and control such factors has important advantage for making progress in the advanced scientific fields.
机译:材料的宏观破损和性质变化通常源自纳米级,一些材料的性质依赖于强烈的温度。因此,对微尺度和纳米技术的传热研究非常重要,以了解和控制温度对材料性质的影响,并且开发先进的测量技术也可以提高我们对此类问题所涉及的理论的知识。由于使用可变温度样本阶段,可利用的温度范围广泛延伸,因此可以观察到温度变化的材料的形貌图像,从而可以进一步研究材料的热性质。因此,应提出传热的理论基础和温度对由于温度变化的隧道电流的影响。在微尺度传热中,本文通过Boltzmann理论将热电流从样品表面传递到探针尖端的问题,这可以通过热传导的双曲线方程来表示几乎相当于松弛时间,比例远大于局部热力学平衡的特征尺度。还分析了探针的热转印模式,并在纸上获得分析溶液。此外,详细讨论了样品温度增量对隧道电流的影响,并且在有限的温度范围内也获得了温度的隧道电流的变化趋势。由于这些因素是可以扰乱样品的地形图像,毫无疑问将产生许多困难来开发新技术,例如通过使用加热和未加热的样品的图像检测微观尺寸的物质的位移和应变。为了理解和控制这些因素对于在高级科学领域取得进展具有重要优势。

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