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Study of the effects of heat-treatment of hydroxyapatite synthesized in gelatin matrix

机译:明胶基质中羟基磷灰石热处理的影响研究

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In the study, the isothermal thermogravimetric analysis (TGA) of hydroxyapatite synthesized in gelatin matrix (HAG) has been performed. 3 wt.% HAG samples were synthesized from the solution simulating the human extracellular fluid (SBF). X-ray diffraction and IR spectroscopy were used to determine the composition. During the experiment, increase in the calcination temperature up to 200°C-800°C was found to cause weight loss. The study of phase composition revealed that heat treatment does not affect the phase composition of the solid phase, which is composed of hydroxylapatite (HA). The prepared HAG (3 wt.% gelatin) samples are shown to have low thermal stability; the degradation of the samples occurs at 400° C.
机译:在该研究中,已经进行了在明胶基质(HAG)中合成的羟基磷灰石的等温热量分析(TGA)。 3重量%。从模拟人细胞外液(SBF)的溶液中合成%HAG样品。使用X射线衍射和IR光谱法测定组合物。在实验期间,发现煅烧温度的增加高达200℃-800℃,导致体重减轻。相对于相组合物的研究表明,热处理不影响固相的相组合物,其由羟基磷灰石(HA)组成。制备的HAG(3重量%的明胶)样品显示出具有低热稳定性;样品的降解发生在400℃。

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