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Preparation and characterization of Fe~(3+)-doped TiO_2/diatomite composite

机译:Fe〜(3 +) - 掺杂TiO_2 /硅藻土复合材料的制备与表征

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Fe~(3+)-doped TiO_2/diatomite composite photocatalyst were prepared by sol-gel method with titanium isopropoxide used as precursor material. The samples were characterized by SEM, XRD, XPS, BET surface area analysis and UV-Vis techniques. The results showed that the optimum concentration of Fe~(3+) in the composite catalyst was 0.2wt% when the quantity of TiO_2 loaded on the diatomite was 30.3wt%. Compared with the un-doped photocatalyst, the Fe~(3+)-doped sample exhibited red shifts of absorption edge and significant enhancement of light absorption at 400~600 nm.
机译:通过溶胶 - 凝胶法制备Fe〜(3 +) - 掺杂的TiO_2 /硅藻土合复合光催化剂用用作前体材料的钛异丙氧化钛制备。样品的特征在于SEM,XRD,XPS,BET表面积分析和UV-VIS技术。结果表明,当硅藻土上负载的TiO_2的量为30.3wt%时,复合催化剂中Fe〜(3+)的最佳浓度为0.2wt%。与未掺杂的光催化剂相比,Fe〜(3 +)掺杂的样品显示出吸收边缘的红色偏移,并在400〜600nm处显着提高光吸收。

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