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Systhesis, Characterization and spectroscopic properties of (2E,6E)-2,6-Bis(2,3,4-tri-methoxy-benzylidene)cyclohexanone

机译:(2E,6E)-2,6-双(2,3,4-三甲氧基苄基)环己酮(2,4-三甲氧基苄基)的合成,表征和光谱性质

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In this paper, (2E,6E)-2,6-Bis(2,3,4-tri-methoxy -benzylidene)cyclohexanone (omitted as tmbcho) (1) was obtained by the reaction of acetic acid, tetrahydrofuran, cyclohexanone and 2,3,4-tri-methoxy-benzaldehyde. Three non-classic hydrogen bonds were observed in the compound. X-ray crystallography shows that the crystal structure is stabilized by intermolecular C-H...π interactions and it contains plenty of conjugated double bonds. The title compound was characterized by UV-vis and fluorescent spectral studies.
机译:本文通过乙酸,四氢呋喃,环己酮和环己酮和环己酮和环己酮及其方法(2E,6E)-2,6-双(2,3,4-三甲氧基 - 苄基)环己酮(省略为TMBCHO)(1)。 2,3,4-三甲氧基 - 苯甲醛。在化合物中观察到三种非经典氢键。 X射线晶体学表明,通过分子间C-H ...π相互作用稳定晶体结构,它含有大量的共轭双键。通过UV-Vis和荧光光谱研究表征标题化合物。

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