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Indomethacin molecular imprinted polymer preparation, characterization of application

机译:吲哚美辛分子印迹聚合物制备,施用表征

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In order to indomethacin (IDM) for imprinting molecular, acrylamide (AA) as functional monomer, ethylene glycol dimethacrylate (EGDMA two) as crosslinking agent, respectively by photopolymerization and thermal polymerization of two methods of aqueous solution polymerization, suspension polymerization preparation of molecularly imprinted polymer. The polymer adsorption experiments show that the use of light-polymerized specificity is strong; light initiated polymer used for sample determination and calibration experiments, results in tap water and river water samples in Enshi Qingjiang indomethacin recoveries were 84.3% and 87.1%, were higher than 80%. Tap water and the relative standard deviation (n = 3) were 3.96%, 14.2%, that can be used for the separation and enrichment of indomethacin in water samples.
机译:为了使分子,丙烯酰胺(AA)作为功能单体,乙二醇二甲基丙烯酸酯(EGDMA两)作为交联剂分别通过光聚合和热聚合,分别通过两种水溶液聚合方法,悬浮聚合制备分子印迹聚合物。聚合物吸附实验表明,使用光聚合的特异性强;用于样品测定和校准实验的光引发的聚合物,导致恩施青江吲哚美辛素回收率的自来水和河水样品为84.3%和87.1%,高于80%。自来水和相对标准偏差(n = 3)为3.96%,14.2%,可用于在水样中分离和富集吲哚美辛。

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