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Multi-walled carbon nanotubes based near-infrared radiation source

机译:基于多壁碳纳米管的近红外辐射源

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Emerging Near-InfraRed (NIR) spectroscopic applications such as biomedical, agrofood, health & beauty and in-line industrial applications require compact and low-cost miniaturized spectrometers. One of the main elements for such devices is the wideband light source, which can be ultimately in the form of an integrated source. In this work, we report a Multi-Walled Carbon Nanotubes (MWCNTs) NIR source for operation with a micro-electro-mechanical system (MEMS) FTIR spectrometer. The source consists of joule micro heater machined on a highly doped silicon substrate, where the heater surrounds an active area. The micro heater is made of a platinum film sputtered on silicon with a thin titanium layer used as an adhesion layer. The chips are singulated then the MWCNTs are plotted in the active area. The SonoPlot® Microplotter II is used to plot a multi-layered 4x4 mm2 MWCNTs thin film with a laser thickness of about 1μm in the active area. A voltage difference is applied to the designated pads on the chip, allowing uniform heating of the square area containing the MWCNTs. The MEMS FTIR spectrometer is used to measure the emitted power spectral density (PSD) from the source with and without the plotting of the MWCNTs thin film. The micro-plotting of the MWCNTs over the silicon substrate improved the PSD recorded by the spectrometer. The reported results show that an engineered light source based on MWCNTs and silicon serves as a good candidate for miniaturized spectrometers.
机译:新兴的近红外(NIR)光谱应用,例如生物医学,农业食品,健康与美容以及在线工业应用,都需要紧凑且低成本的小型化光谱仪。这种设备的主要元素之一是宽带光源,宽带光源最终可以采用集成光源的形式。在这项工作中,我们报告了一种多壁碳纳米管(MWCNT)NIR源,可用于微机电系统(MEMS)FTIR光谱仪。源包括在高掺杂硅衬底上加工的焦耳微加热器,加热器围绕着有效区域。微型加热器由溅射在硅上的铂膜制成,该铂膜具有用作粘合层的薄钛层。将芯片切单,然后将MWCNT绘制在有效区域中。 SonoPlot®Microplotter II用于在有源区域中绘制激光厚度约为1μm的多层4x4 mm2 MWCNTs薄膜。将电压差施加到芯片上的指定焊盘,从而均匀加热包含MWCNT的正方形区域。 MEMS FTIR光谱仪用于测量有无MWCNTs薄膜的情况下从源发射的功率谱密度(PSD)。 MWCNT在硅衬底上的微图谱改善了由分光光度计记录的PSD。报告的结果表明,基于MWCNT和硅的工程光源可作为微型光谱仪的理想选择。

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