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Influences of pretreatment solution concentrations on copper-doped SiC particles made through electroless plating technique

机译:预处理溶液浓度对化学镀铜掺杂SiC颗粒的影响

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Pretreatments for copper-doped SiC particles made by an electroless-plating technique, the preconditions to attain good coatings, were conducted in order to obtain the active and clean surface of SiC particles. An orthogonal experiment method was used to determine the concentration of every pretreatment solution. The morphologies of the coatings were observed in a scanning electronic microscope(SEM), the composition of the coatings was analyzed by an energy-dispersive X-ray analysis (EDS), and the phases in the coatings were identified by a X-ray differtometer (XRD). The influences of pretreatment solution concentrations on the copper coatings quality of SiC particles were dealt with. The results showed that the pretreatment solution concentrations had great influences on the coatings quality of SiC particles. The obvious effects on the copper coatings derived from the coarsening solution concentration. The optimized copper coatings of SiC particles were uniform and dense, no bare SiC particles were seen and the interfaces between SiC and Cu bonded well. The high quality and low cost coatings were also obtained after the expensive PaCl2 activating agent had been substituted for AgNO3.
机译:为了获得活性和清洁的SiC颗粒表面,对通过化学镀技术制备的掺杂铜的SiC颗粒进行了预处理,以达到获得良好涂层的前提。使用正交实验方法确定每种预处理溶液的浓度。在扫描电子显微镜(SEM)中观察涂层的形貌,通过能量色散X射线分析(EDS)分析涂层的组成,并通过X射线差示仪鉴定涂层中的相。 (XRD)。研究了预处理溶液浓度对SiC颗粒镀铜质量的影响。结果表明,预处理溶液浓度对SiC颗粒的涂层质量影响很大。粗化液浓度对铜镀层有明显的影响。优化后的SiC颗粒铜涂层均匀且致密,未见裸露的SiC颗粒,且SiC与Cu之间的界面良好结合。在用昂贵的PaCl2活化剂代替AgNO3之后,也获得了高质量和低成本的涂层。

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