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CATALYST-FREE ELECTROCHEMICAL DEUTERATION METHOD USING DEUTERIUM OXIDE AS DEUTERIUM SOURCE
CATALYST-FREE ELECTROCHEMICAL DEUTERATION METHOD USING DEUTERIUM OXIDE AS DEUTERIUM SOURCE
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机译:使用氧化氘作为氘源的无催化剂电化学氘化方法
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摘要
A catalyst-free electrochemical deuteration method using deuterium oxide as a deuterium source, adding an electrolyte, an organic compound containing an ethylenic bond or acetylenic bond, deuterium oxide, and an organic solvent into a reactor, applying a direct current voltage of 4-8 V between electrodes of a carbon felt in an atmosphere of an inert gas for an electrolytic reaction, to obtain a product, and purifying the product to obtain a deuterated product. In the method provided by the present disclosure, with the organic compound containing an ethylenic bond or acetylenic bond as a raw material, deuterium oxide as a deuterium source, cheap and readily available carbon electrode materials as cathodes and anodes, it is possible to obtain deuterated products by a direct current electrolysis in an organic solvent, without any transition metal catalysts.
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