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SYSTEM AND METHOD FOR SCALED-UP SYNTHESIS OF DOPED AND FUNCTIONALIZED GRAPHENE DERIVATIVES THROUGH MECHANICAL EXFOLIATION PROCESS

机译:通过机械剥离过程进行缩小合成掺杂和官能化石墨烯衍生物的系统和方法

摘要

The embodiments herein provide method and system for synthesizing graphene and a plurality of derivatives through a mechanical shearing process. The method comprises synthesizing a ceramic substrate from a ceramic material in particulate form; depositing carbon material on the synthesized ceramic substrate to synthesize graphene ceramic substrate coated with carbonaceous material; dissolving/dispersing the graphene ceramic substrate coated with carbonaceous material in one solvent and perform mechanical shearing to obtain a dispersion solution of graphene and its derivatives. This graphene dispersions is further subjected to ultrasonication to obtain graphene nano-platelets. The embodiments also provide mechanical exfoliation method for the bulk synthesis of doped and functionalized graphene nano-platelets. The doped graphene ceramic composite are subjected to exfoliation with or without simultaneous ultra-sonication for obtaining doped graphene sheet. The exfoliated graphene sheets obtained from doped graphene ceramic composite are subjected to ultra-sonication and centrifugation.
机译:本文的实施方案提供了用于通过机械剪切工艺合成石墨烯和多种衍生物的方法和系统。该方法包括将陶瓷基材从颗粒形式的陶瓷材料合成;沉积在合成的陶瓷基材上的碳材料,合成涂有碳质材料的石墨烯陶瓷基材;将带有碳质材料的石墨烯陶瓷基材溶解/分散在一种溶剂中并进行机械剪切以获得石墨烯及其衍生物的分散溶液。该石墨烯分散体进一步进行超声波以获得石墨烯纳米血小板。实施例还提供了用于掺杂和官能化的石墨烯血小板的体积合成的机械剥离方法。将掺杂的石墨烯陶瓷复合材料与用于获得掺杂的石墨烯片的同时超声检查进行剥离。从掺杂的石墨烯陶瓷复合物中获得的剥离石墨烯片经受超超声处理和离心。

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