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Aluminum oxynitride having improved optical characteristics and method of manufacture

机译:具有改善的光学特性的氧氮化铝及其制造方法

摘要

A method of preparing substantially homogeneous aluminum oxynitride powder is provided comprising the steps of reacting gamma aluminum oxide with carbon in the presence of nitrogen, and breaking down the resulting powder into particles in a predetermined size range. PPA method of preparing a durable optically transparent body from this powder is also provided comprising the steps of forming a green body of substantially homogeneous cubic aluminum oxynitride powder and sintering said green body in a nitrogen atmosphere and in the presence of predetermined additives which enhance the sintering process. Preferred additives are boron, in elemental or compound form, and at least one additional element selected from the group of yttrium and lanthanum or compounds thereof. The sintered polycrystalline cubic aluminum oxynitride has a density greater than 99% of theoretical density, an in-line transmission of at least 50% in the 0.3-5 micron range, and a resolving angle of 1 mrad or less.
机译:提供了一种制备基本均匀的氮氧化铝粉末的方法,该方法包括以下步骤:使γ氧化铝与碳在氮的存在下反应,并将所得粉末分解成预定尺寸范围的颗粒。还提供了由这种粉末制备耐用的光学透明体的步骤,该步骤包括形成基本均匀的立方氮氧化铝粉末的生坯,并在氮气氛中和在预定的添加剂存在下烧结所述生坯的步骤,所述添加剂可增强烧结过程。优选的添加剂是元素形式或化合物形式的硼,以及选自钇和镧或其化合物中的至少一种其他元素。烧结的多晶立方氮化铝铝的密度大于理论密度的99%,在线透射率在0.3-5微米范围内至少为50%,且分辨角为1毫拉德或更小。

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