首页> 外国专利> Procedure for racemizar HYDROLYZE esters and alkyl acid (-) - 2 - (4 - difluormetoxifenil metilbutirico) - 3.

Procedure for racemizar HYDROLYZE esters and alkyl acid (-) - 2 - (4 - difluormetoxifenil metilbutirico) - 3.

机译:消旋异氰酸酯和烷基酸(-)-2-(4--difluormetoxifenil metilbutirico)-3。

摘要

Procedure for racemizar HYDROLYZE esters and alkyl acid (-) - 2 - (4 - difluorometoxifenil metilbutirico) - 3 - with one to two molar Equivalents of sodium or Potassium Hydroxide, in the presence of C1 - C3 anhydrous alcohol, at a temperature of 60 to 100 or the Boiling Point of methanol during A time period of 2 to 10 hours until the Reaction is essentially complete.The resulting Racemic acid was resolved into its components by means of optically Active salts prepared from the Racemic acid with optically active amines and subsequent Recovery of the Dextro rotatory isomer desired. It is used to prepare type pyrethroid pesticides.
机译:在60至60°C的温度下,在C1-C3无水醇存在下,用1至2摩尔当量的氢氧化钠或氢氧化钾,消旋地水解酯和烷基(-)-2-(4--二氟甲氧基苯甲腈)的方法在2至10个小时内直至反应完全完成的过程中达到100或甲醇的沸点。通过消旋酸与旋光胺合成的旋光盐将所得消旋酸分解成其组分需要恢复Dextro旋转异构体。用于制备拟除虫菊酯类农药。

著录项

  • 公开/公告号ES8602592A1

    专利类型

  • 公开/公告日1986-03-16

    原文格式PDF

  • 申请/专利权人 AMERICAN CYANAMID COMPANY;

    申请/专利号ES19850540795

  • 发明设计人

    申请日1985-02-28

  • 分类号C07C69/734;

  • 国家 ES

  • 入库时间 2022-08-22 07:37:39

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