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SOLUTION PROCESS FOR PREPARING METAL SALT ESTERS OF HYDROCARBYL SUBSTITUTED SUCCINIC ACID OR ANHYDRIDE AND ALKANOLS
SOLUTION PROCESS FOR PREPARING METAL SALT ESTERS OF HYDROCARBYL SUBSTITUTED SUCCINIC ACID OR ANHYDRIDE AND ALKANOLS
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机译:制备氢取代的琥珀酸或酸酐和链烷烃金属盐酯的解决方法
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摘要
A solution process is disclosed for preparing a solubilized metal salt ester by reacting an ester compound, such as 2,2'-thiodiethyl-bis (octadecenyl) succinate ester, with a metal carboxylate, such as calcium acetate, in the process of a mixture of (a) a first co-solvent and/or third co-solvent, such as toluene and/or dodecylbenzene respectively, and (b) a second co-solvent such as methanol, to form the metal salt ester product and an effluent mixture of an acid, such as acetic acid, optional co-solvent first, and second co-solvent, followed by the optional addition of a third co-solvent, and vacuum distilling the resulting mixture to remove the effluent mixture to produce a solution of the product and third co-solvent.
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