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PLANETARY CENTRIFUGE FOR COUNTER-CURRENT CHROMATOGRAPHY

机译:逆流色谱的行星离心

摘要

FIELD: equipment hor high-speed counter-current chromatography; analytical chemistry for semi-preparative and analytical separation of organic, bioorganic and inorganic compounds close by properties. SUBSTANCE: planetary centrifuge has housing where the following components are arranged: hollow shaft engageable with engine, carrier disc fitted on shaft, chromatographic separation unit secured on axles mounted rotatably on carrier disc and connected with gear train; centrifuge is also provided with balancing system, swivel support and relief damper; balancing system is made in the form of upright mounted coaxially inside shaft on base of housing in spherical support and hinge suspension mounted on upper end of upright and rigidly connected with shaft; rotor of engine is mounted coaxially on outer side of shaft; stator is secured on base of housing by means of flexible member; gear train is engageable with base of housing which is secured on support; relief damper is made in the form of bracket with profiled groove rigidly connected with upright for turn about it; groove is engageable with base of housing through flexible member; chromatographic separation unit contains n drums secured on axles coaxially relative to one another, n tubes wound on drums and 2n solution supply and discharge mains connected with tubes both in series and in parallel; n is even number. EFFECT: extended functional capabilities due to possibility of performing several independent separation processes simultaneously; enhanced reliability and efficiency of separation of samples due to reduction of vibration at simultaneous of rotational speed and installation of centrifuge at any angle relative to horizontal plane without disassembly. 2 cl, 3 dwg
机译:领域:高速逆流色谱仪设备;用于根据化学性质对有机,生物有机和无机化合物进行半制备和分析分离的分析化学。实质:行星式离心机的外壳布置有以下部件:可与发动机接合的空心轴,安装在轴上的承载盘,固定在可旋转地安装在承载盘上并与齿轮系连接的轴上的色谱分离单元;离心机还配有平衡系统,旋转支撑和泄压风门;平衡系统的形式是:立柱形式,同轴安装在轴的内部,球形轴承座位于壳体的底部;铰链悬架,安装在立柱的上端,与轴刚性连接。发动机的转子同轴安装在轴的外侧。定子通过柔性件固定在壳体的基座上。齿轮系可与固定在支撑件上的外壳底部啮合;泄压风门以支架形式制成,其轮廓槽与立柱牢固地连接以绕其转动;凹槽通过柔性构件与壳体的底部接合。色谱分离单元包括:n个彼此相对同轴地固定在轴上的鼓,n个缠绕在鼓上的管以及2n个与管串联和并联连接的溶液供,输总管。 n是偶数。效果:由于可以同时执行多个独立的分离过程,因此扩展了功能能力;由于在降低转速的同时降低了振动并在不拆卸的情况下相对于水平面以任意角度安装了离心机,从而提高了样品分离的可靠性和效率。 2 cl,3 dwg

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