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Field-portable supercritical CO.sub.2 extractor

机译:现场便携式超临界CO.sub.2萃取器

摘要

The present invention is an apparatus for extracting organic compounds from solid materials. A generator vessel has a removable closure for receiving a solid or liquid solvent which is heated with a resistive heating element to a gaseous or supercritical phase. The removable closure is unencumbered because the side wall is penetrated with an outlet for the gaseous or supercritical solvent. The generator vessel further has a pressure transducer that provides an electronic signal related to pressure of the gaseous or supercritical solvent. The apparatus of the present invention further includes at least one extraction cell having a top and a bottom and a wall extending therebetween, wherein the bottom is sealably penetrated by an inlet for gaseous or supercritical solvent received through a manifold connected to the outlet, the top having an easy-open removable closure cap, and the wall having an outlet port. Finally, a permeable sample cartridge is included for holding the solid materials and to provide radial-flow of the extraction fluid, which is placed within the extraction cell.
机译:本发明是一种从固体材料中提取有机化合物的设备。发电机容器具有用于接收固体或液体溶剂的可移除的封闭件,该固体或液体溶剂被电阻式加热元件加热至气相或超临界相。可移动的封盖不受阻碍,因为侧壁上有用于气态或超临界溶剂的出口。发生器容器还具有压力传感器,该压力传感器提供与气态或超临界溶剂的压力有关的电子信号。本发明的设备还包括至少一个具有顶部和底部以及在其间延伸的壁的萃取室,其中底部通过用于通过连接到出口的歧管接收的气态或超临界溶剂的入口密封地穿透。具有易于打开的可移动封闭盖,并且壁具有出口。最后,包括一个可渗透的样品盒,用于容纳固体材料并提供提取液的径向流动,该流体被置于提取室中。

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