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Process for the production of Monoglyceride based on glicerolisis methyl ester

机译:基于甘油酸甘油酯的甘油单酸酯的生产方法

摘要

The Invention discovers a process for the production of mono methyl ester derivatives by glicerolisis fat and Animal and vegetable oils which includes mixing a surplus of 0.1 to 3 moles of glycerol in the Methyl Ester, subjected to the Reaction mixture to a temperature of between 130 to 160 in a vacuum of 200 to 400 m Bar, adding Alkaline Catalysts.Stopping the Reaction by efriamiento Rapid mixing rezcciu00f3n and destruction of alkaline Catalyst when the amount of Glycerides has reached a concentration of mono and diglyceridesFrom 10 to 60%.Leaving The Catalyst into the mixture of rezzciu00f3n to catalyze The reaction of water in a separate reactor excess methyl ester and glycerol by stopping the Reaction by distillation enfriamieHow quickly The reaction Mixture with alkaline Catalyst and the destruction of the Reactor when the amount of Glycerides has reached a concentration of 40 to 60% and the radius of concentrations of MOno and diglicu00e9ridas are between 3 to 10.
机译:本发明发现了一种由滑脂脂肪和动植物油生产单甲酯衍生物的方法,该方法包括在反应混合物中将过量的0.1至3摩尔甘油混合在甲基酯中,使反应混合物的温度在130至130℃之间。 160在200至400 m Bar的真空中,添加碱性催化剂。通过efriamiento停止反应当甘油酯的含量达到甘油单酯和甘油二酯的浓度从10%到60%时,快速混合rezcci u3f和破坏碱性催化剂。催化剂进入rezzci的混合物中以催化反应在另一个反应器中通过停止蒸馏反应停止反应中多余的甲酯和甘油中的水的反应反应多快与碱性催化剂混合并在达到甘油酯量时破坏反应器浓度为40%到60%,MONo和diglic浓度的半径在3到10之间。

著录项

  • 公开/公告号ECSP982559A

    专利类型

  • 公开/公告日2000-05-25

    原文格式PDF

  • 申请/专利权人

    申请/专利号EC1998SP02559

  • 发明设计人 WOZNY GUENTER;JEROMIN LUTZ;LI PU;

    申请日1998-06-26

  • 分类号C07C305/10;

  • 国家 EC

  • 入库时间 2022-08-22 01:56:34

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