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Process for obtaining of microcrystalline cellulose

机译:获得微晶纤维素的方法

摘要

The invention relates to the chemical technology, in particular to the processes for obtaining of microcrystalline cellulose. Summary of the invention consists in that the cellulose-containing raw material is preliminarily dried and comminuted. Afterwards, it is impregnated with 10% NaOH solution in the ratio solid substance : solution 1 : 4_6 within 5_6 hours, then the solution is removed. The obtained mass is treated with 1% NaOH solution in the ratio solid substance : solution 1 : 6 at a temperature of 75 degree C within 24 hours. The NaOH solution is removed, and the obtained mass is treated with chlorinated water in 3 stages, then it is washed with water and it is treated with 1% NaOH solution within 1,5_2,5 h, which it is removed afterwards, and the obtained substance is washed. Then within 15 min at a temperature of 105 degree C it is treated with HCl 5N solution. The obtained special-purpose product is washed, filtered, dried and pulverized.Claims: 5
机译:本发明涉及化学技术,尤其涉及获得微晶纤维素的方法。发明内容在于,将含纤维素的原料预先干燥并粉碎。之后,在5_6小时内以固体物质:溶液1:4_6的比例浸渍10%NaOH溶液,然后将溶液除去。在75℃的温度下,在24小时内用固体物质:溶液1∶6的比例的1%NaOH溶液处理得到的物质。除去NaOH溶液,将所得物料用氯化水分3个阶段处理,然后用水洗涤,并在1,5_2,5 h内用1%NaOH溶液处理,然后将其除去。将获得的物质洗涤。然后在15分钟内在105摄氏度的温度下用HCl 5N溶液处理。洗涤,过滤,干燥和粉碎所得专用产品。索赔:5

著录项

  • 公开/公告号MD1923F1

    专利类型

  • 公开/公告日2002-05-31

    原文格式PDF

  • 申请/专利权人 CIBOTARI SILVIA;

    申请/专利号MD20010000316

  • 发明设计人 DIUG EUGEN;CIBOTARI SILVIA;

    申请日2001-09-26

  • 分类号C08B15/00;C08B15/02;

  • 国家 MD

  • 入库时间 2022-08-22 00:44:38

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