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SYSTEM FOR THE PRODUCTION OF COMPLEX POLYESTER USING AN ESTHERIFICATION REACTOR WITHOUT MIXING

机译:使用不带混合反应器的合成反应器生产复杂聚酯的系统

摘要

1. A method for esterification of the reaction medium, comprising the steps of:! (a) subjecting the esterification reaction medium to a vertically elongated esterification reactor, said esterification reactor forming one vessel having a fluid inlet and at least two separate outlets containing a liquid outlet through which the reaction medium is discharged the specified reactor for esterification, and the exit for steam through which the vaporous by-product of esterification is discharged from the reactor for esterification, and the specified exit for steam is located on the same tank for pain higher than the specified outlet for the liquid, and wherein said esterification reactor provides heat to the reaction medium within itself; and! (b) said reaction medium in said esterification reactor is not mechanically stirred, or if mechanically mixed, less than about 50% of said stirring of the reaction medium is provided by mechanical stirring. ! 2. The method according to claim 1, wherein the reaction medium entering the fluid inlet has an initial conversion of at least about 70%. ! 3. The method of claim 2, wherein the reaction medium discharged through the liquid outlet has a final conversion of at least about 80%. ! 4. The method according to claim 3, in which the specified initial conversion is at least about 75% and the specified final conversion is at least about 85%. ! 5. The method according to claim 1, wherein said esterification reactor has a height to diameter ratio ranging from about 1.15: 1 to about 10: 1. ! 6. The method according to claim 1, wherein said esterification reactor
机译:1.一种反应介质的酯化方法,包括以下步骤: (a)使酯化反应介质经受垂直延伸的酯化反应器,所述酯化反应器形成一个容器,该容器具有流体入口和至少两个单独的出口,所述出口包含液体出口,反应介质通过所述液体出口排出指定的用于酯化的反应器,蒸汽出口,酯化反应的蒸气副产物通过该蒸汽出口从酯化反应器中排出,蒸汽的指定出口位于同一罐中,其痛苦高于液体的出口,并且其中所述酯化反应器提供热量自身的反应介质;和! (b)不机械搅拌所述酯化反应器中的所述反应介质,或者如果机械混合,则通过机械搅拌提供少于约50%的所述反应介质搅拌。 ! 2.根据权利要求1所述的方法,其中进入所述流体入口的所述反应介质具有至少约70%的初始转化率。 ! 3.权利要求2的方法,其中通过液体出口排出的反应介质的最终转化率为至少约80%。 ! 4.根据权利要求3所述的方法,其中,所述指定的初始转化率为至少约75%,并且所述指定的最终转化率为至少约85%。 ! 5.根据权利要求1的方法,其中所述酯化反应器的高度与直径之比为约1.15∶1至约10∶1。 6.根据权利要求1的方法,其中所述酯化反应器

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