首页> 外国专利> Transparent conductive thin film and method of manufacturing the same amorphous, as well as, sputtering target and method of manufacturing the same in order to obtain a transparent conductive thin film of amorphous

Transparent conductive thin film and method of manufacturing the same amorphous, as well as, sputtering target and method of manufacturing the same in order to obtain a transparent conductive thin film of amorphous

机译:透明导电薄膜及其制造方法,以及非晶靶的制造方法,溅射靶及其制造方法

摘要

There is provided an amorphous transparent conductive thin film with a low resistivity, a low absolute value for the internal stress of the film, and a high transmittance in the visible light range, an oxide sintered body for manufacturing the amorphous transparent conductive thin film, and a sputtering target obtained therefrom. An oxide sintered body is obtained by: preparing InSUB2/SUBOSUB3 /SUBpowder, WOSUB3 /SUBpowder, and ZnO powder with an average grain size of less than 1 mum so that tungsten is at a W/In atomic number ratio of 0.004 to 0.023, and zinc is at a Zn/In atomic number ratio of 0.004 to 0.100; mixing the prepared powder for 10 to 30 hours; granulating the obtained mixed powder until the average grain size is 20 to 150 mum; molding the obtained granulated powder by a cold isostatic press with a pressure of 2 to 5 ton/cmSUP2/SUP, and sintering the obtained compact at 1200 to 1500 degree.C. for 10 to 40 hours in an atmosphere where oxygen is introduced into the atmosphere of the sinter furnace at a rate of 50 to 250 liters/min per 0.1 mSUP3 /SUPfurnace volume.
机译:本发明提供一种电阻率低,膜的内应力的绝对值低,可见光范围的透射率高的非晶态透明导电性薄膜,用于制造该非晶态透明导电性薄膜的氧化物烧结体,以及由此获得的溅射靶。通过以下方法获得氧化物烧结体:制备In 2 O 3 粉末,WO 3 粉末和平均粒径小于ZnO的粉末小于1μm,使得钨的W / In原子数比为0.004至0.023,并且锌的Zn / In原子数比为0.004至0.100;将制备的粉末混合10至30小时;将得到的混合粉末造粒,直至平均粒径为20〜150μm。通过冷等静压机在2至5吨/ cm 2 的压力下模压所得粒状粉末,并在1200至1500℃下烧结所得压块。在将氧气以每0.1 m 3 炉体积的50至250升/分钟的速率引入烧结炉气氛中的气氛中保持10至40小时。

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