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METHOD FOR THE CONTINUOUS SYNTHESIS OF MONOALKYL-HYDRAZINES WITH A FUNCTIONALIZED ALKYL GROUP

机译:连续合成功能性烷基单烷基肼的方法

摘要

The invention monoalkylamino having a functionalized alkyl group relates to a continuous method for the synthesis of hydrazine. The method of the present invention, by the addition of anhydrous sodium hydroxide, an monoalkyl synthesized by anhydrous amine mono chlor amine and the reaction will be a solution containing a hydrazine characterized in that it comprises the steps consisting of that di mixing with the organic phase and the water . The invention thereof di- can be used to obtain a complete selectivity with respect to the hydrazine, and tri-alkyl mono without the presence of a substituted form. According to the present invention, the unreacted starting amine is collected and is directly reused without any further treatment.
机译:具有官能化烷基的本发明的单烷基氨基涉及合成肼的连续方法。通过添加无水氢氧化钠,由无水胺单氯胺合成的单烷基,本发明的方法将成为含有肼的溶液,其特征在于其包括以下步骤:与有机相二混合还有水。本发明的di-可用于获得相对于肼和三烷基单酯的完全选择性,而没有取代形式的存在。根据本发明,未反应的起始胺被收集并且无需任何进一步处理就可以直接重复使用。

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