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METHOD FOR IDENTIFYING SUNFLOWER OIL BASED ON LINOLIC OR OLEIC TYPE THEREOF

机译:基于线性或油型的葵花籽油识别方法

摘要

FIELD: chemistry.;SUBSTANCE: in the method, which involves collecting a (6.00±0.2) g oil sample, after collection, the oil sample is prepared by temperature control at (-8±0.2)°C for 1 hour, after which the oil sample is put into a the sensor of a pulsed NMR analyser, the signal amplitude of NMR triacylglycerine protons which are in liquid phase, the first (A1), second (A2) and third (A3) component in percentages and the spin-spin relaxation time of triacylglycerine protons which are in liquid phase, the first (T21), second (T22) and third (T23) component in milliseconds are measured and the average value of the spin-spin relaxation time (T2SR) in milliseconds is calculated using the formula:; ;The linolic type of sunflower oil is indicated by the value of T2SR ranging from 28 to 32 milliseconds, and the oleic type is indicated by the value of T2SR ranging from 8 to 12 milliseconds.;EFFECT: simple, faster and safer analysis.;2 ex
机译:领域:化学。实质:该方法涉及收集(6.00±0.2)g的油样,收集后,通过在(-8±0.2)°C的温度下控制1小时来制备油样,然后将油样放入脉冲NMR分析仪的传感器中,液相中的NMR三酰基甘油质子的信号幅度,第一个(A 1 ),第二个(A 2 < / Sub>)和第三个(A 3 )成分的百分比以及处于液相中的三酰甘油质子的自旋自旋弛豫时间,第一个(T 21 ),测量第二(T 22 )和第三(T 23 )分量(以毫秒为单位),并测量自旋-自旋弛豫时间的平均值(T 2SR )(以毫秒为单位),可使用以下公式计算: ;葵花籽油的亚油酸类型由T 2SR 的值表示,范围为28至32毫秒,油酸类型由T 2SR 的值指示。 8到12毫秒;效果:简单,快速,安全的分析。; 2 ex

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