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Method for determining a residual stress gradient in a sample

机译:确定样品中残余应力梯度的方法

摘要

The present invention relates to a method for determining a residual stress gradient in a sample using X-ray diffraction, wherein the sample is supported on a sample holder defining a sample plane, the method comprising the steps of- irradiating a beam from an X-ray source onto the sample and detecting a beam diffracted by the sample with an X-ray detector having two degrees of freedom, wherein the directions of the incident beam and/or the diffracted beam are varied in relation to the sample and the position of the X-ray detector is varied in two degrees of freedom, and- determining the values sin2Ψ and τµ, which are representative for the residual stress gradient in the sample, as a function of the X-ray source and x-ray detector positions taking into account the two degrees of freedom of the detector, wherein Ψ is the polar angle, τ is the penetration depth of the beam into the sample, and µ is the mass attenuation coefficient of the sample.;In order to improve this method, it is suggested that the variation of the directions of the incident beam and/or the diffracted beam comprises a rotation of the diffracted beam by an angle 2θχ within a plane that is inclined against the sample plane, designated in-plane arm rotation.
机译:本发明涉及一种使用X射线衍射确定样品中残余应力梯度的方法,其中将样品支撑在限定样品平面的样品架上,该方法包括以下步骤:-将来自X射线源的光束照射到样品上,并使用具有两个自由度的X射线检测器检测由样品衍射的光束,其中入射光束和/或衍射光束的方向相对变化样品和X射线检测器的位置在两个自由度中变化,并且-在考虑两个角度的情况下,确定代表样品中残余应力梯度的值sin 2 Ψ和τµ,作为X射线源和X射线探测器位置的函数探测器的自由度,其中Ψ是极角,τ是光束进入样品的穿透深度,μ是样品的质量衰减系数。;为改进此方法,建议改变入射光束和/或衍射光束的方向的“旋转”包括衍射光束在相对于样品平面倾斜的平面内以角度2θx旋转,称为平面内臂旋转。

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