首页> 外国专利> PROCESS FOR PRODUCING MESOPHASE PITCH BY HYDROGENATION OF HIGH-TEMPERATURE COAL TAR

PROCESS FOR PRODUCING MESOPHASE PITCH BY HYDROGENATION OF HIGH-TEMPERATURE COAL TAR

机译:高温煤焦油加氢制备中间相沥青的方法

摘要

The present invention is directed to the process of producing mesophase pitch by hydrogenation of high temperature coal tar, removing salts and insoluble quinoline from high temperature coal tar to obtain a pure oil; Use of pure oil as the hydrogenation feed oil, or pre-distillation of the pure oil to obtain a bottom component with a boiling point above 230 0 C and forming the bottom component into a hydrogenation feed oil; Purifying said hydrogenation feed oil by catalytic hydrogenation to obtain a purified hydrogenated oil; Distilling the purified hydrogenated oil to obtain a hydrogenated pitch; And thermal condensation polymerization of the hydrogenated pitch to obtain mesophase pitch. This process makes it easy to control the degree of hydrogenation, to completely remove impurities, to improve the dispersibility of the raw materials, to be insensitive to carbon deposition and coking during the process, and to prevent clogging of the reactor. The product has a high mesophase pitch content, a low softening point and a low impurity content.
机译:本发明涉及通过高温煤焦油的氢化来生产中间相沥青,从高温煤焦油中除去盐和不溶性喹啉以得到纯油的方法。使用纯油作为加氢进料油,或对纯油进行预蒸馏,得到沸点高于230 0℃的塔底组分并将该塔底组分形成加氢进料油;通过催化加氢提纯所述加氢原料油,得到提纯的加氢油;蒸馏纯化的氢化油以获得氢化沥青;然后进行热缩聚反应得到氢化沥青的中间相沥青。该方法使得易于控制氢化程度,完全除去杂质,提高原料的分散性,在该过程中对碳沉积和焦化不敏感并且防止反应器堵塞。该产物具有高中间相沥青含量,低软化点和低杂质含量。

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