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METHOD FOR STRONTIUM HEXAFERRITE NANOPARTICLES PREPARATION

机译:六方锶酸锶纳米粒子的制备方法

摘要

FIELD: chemistry.;SUBSTANCE: method for strontium hexaferrite nanoscale particles production includes mixing of a strontium nitrate solution in distilled water with a ferric nitrate solution in glycerol and distilled water solution to achieve the atomic ratio Sr/Fe=1:10, continuous heating and stirring at 50°C for one hour, addition of ammonia and polyethylene glycol in a ratio of 5:1, stirring of the resulting mixture at 80°C for 8 hours and centrifuging at a speed of 11000 rpm, calcination at 450°C for 1.5 hours, and sintering at 1000-1100 °C, all heating and stirring processes are conducted under the influence of continuous ultrasonic irradiation with frequency of 10-25 kHz.;EFFECT: increased homogeneity of strontium hexaferrite nanoparticles size.;3 ex
机译:六锶锶铁氧体纳米级粒子的制备方法:将蒸馏水中的硝酸锶溶液与甘油和蒸馏水溶液中的硝酸铁溶液混合,以达到原子比Sr / Fe = 1:10,并连续加热在50℃下搅拌1小时,以5∶1的比例加入氨和聚乙二醇,在80℃下将所得混合物搅拌8小时,并以11000rpm的速度离心,在450℃下煅烧。持续1.5小时,并在1000-1100°C下烧结,所有加热和搅拌过程均在连续超声波辐射的影响下进行,频率为10-25 kHz;效果:六铁酸锶纳米粒子尺寸的均匀性增加; 3 ex

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