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Synthesis of nanoparticles of strontium hexaferrite by co precipitation method from homogeneous solutions

机译:共沉淀法从均相溶液中合成六铁酸锶纳米粒子

摘要

the invention relates to the synthesis of nanoparticles of strontium heksaferita (srfe12o19) with the method soobarjanja from homogeneous solutions, with a narrow size distribution in the range of 40 to 100 nm, the thermal treatment in the temperature range between nanoparticles synthesised 600 degrees c and 1100 degrees c t er specific magnetizacijo sigma - in the area between 64 and 67 am2 / kg,remanentno magnetizacijo mri in the range between 6 and 39 am2 / kg and koercitivnostjo in the range between 150 and 5400 oe, the precipitation of water obarjanjavodnih solutions of sulfates, chlorides and nitrates sr2 + metal ions, fe2 +, fe3 + with aqueous solutions of alkali obarjalnih reagents nh4oh, naoh, na2co3, co (nh2) 2 and (c4h13no), at ph values in the range between 7 and 14.in the temperature range between 20 degrees c and 30 degrees c, and the time to maximum temperature restraint from 30 to 120 minutes, the technology of surface treatment of nanoparticles synthesised with water solution of ethanol in a ratio of 1: 1.the technology of drying surface treated nanoparticles in temperaturnemobmou010dju from 100 degrees c to 120 degrees c and the maximum temperature restraint time of 120 minutes to 480 minutes and technology of heat treatment surface treatment of nanoparticles in the temperature range from 400 degrees c, d about 1100 degrees c in air atmosphere by keeping the peak temperature in the range from 60 to 360 minutes of menut adapted to conditions of unwanted and harmful electromagnetic radiation in the area of health milimetrskem electromagnetic waves at different podrou010djihelektrotehnike, construction and in the field of ecology and environmental protection.
机译:本发明涉及用均相溶液(soobarjanja)从均相溶液中合成heksaferita(srfe12o19)纳米粒子的方法,该纳米粒子具有在40至100nm范围内的窄尺寸分布,在600℃至200℃之间在温度范围内进行热处理。 1100 ct er比磁化强度σ-在64至67 am2 / kg之间的区域,remanentno magnetizacijo mri在6至39 am2 / kg的范围内,koercitivnostjo在150至5400 oe的范围内,水的沉淀obarjanjavodnih硫酸盐,氯化物和硝酸盐sr2 +金属离子,fe2 +,fe3 +与碱性obarjalnih试剂nh4oh,naoh,na2co3,co(nh2)2和(c4h13no)的水溶液的溶液,pH值在7和14之间在20摄氏度到30摄氏度之间的温度范围内,达到最大温度限制的时间为30到120分钟,水合成纳米颗粒的表面处理技术1:1比例的乙醇溶液的干燥工艺在100℃至120℃的温度下进行表面处理的纳米粒子的干燥工艺和120℃至480分钟的最大温度限制时间的热处理工艺。通过将峰值温度保持在60至360分钟的菜单范围内,使其在空气中的温度范围在400摄氏度至1100摄氏度之间,以适应健康milimetrskem电磁波区域中有害和有害的电磁辐射的条件在不同的podro u010djihelektrotehnike,建筑以及生态和环境保护领域。

著录项

  • 公开/公告号SI23891A

    专利类型

  • 公开/公告日2013-03-29

    原文格式PDF

  • 申请/专利权人 NANOTESLA INSTITUT;CO NAMASTE;

    申请/专利号SI20110000353

  • 发明设计人 ANDREJ ZNIDARSIC;ANA DRMOTA PETRIC;

    申请日2011-09-08

  • 分类号H01F1/00;B82B3/00;C01F1/00;

  • 国家 SI

  • 入库时间 2022-08-21 16:40:02

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