首页> 外国专利> CONTINUOUS SYNTHESIZING METHOD OF CORE SHELL STRUCTURE NANOPARTICLE WITH METAL CORE AND OXIDE SHELL, CONTINUOUS SYNTHESIZING DEVICE AND CORE SHELL STRUCTURE NANOPARTICLE

CONTINUOUS SYNTHESIZING METHOD OF CORE SHELL STRUCTURE NANOPARTICLE WITH METAL CORE AND OXIDE SHELL, CONTINUOUS SYNTHESIZING DEVICE AND CORE SHELL STRUCTURE NANOPARTICLE

机译:具有金属核和氧化物壳的核壳结构纳米粒子的连续合成方法,连续合成装置和核壳结构纳米粒子

摘要

PROBLEM TO BE SOLVED: To provide a method and a device for continuously synthesizing a nanoparticle with less process without generating variation of particle diameter or aggregation, and a core shell structure nanoparticle.;SOLUTION: There is related to a continuous synthesizing method of a core shell structure nanoparticle including: continuously synthesizing a metal nanoparticle with diameter of 1 to 100 nM with a circulation type reactor 3 in pre-stage including at least one step circulation type reactor, and hydrolyzing an oxide precursor in a circulation type reactor 10 in a subsequent-stage including at least one step circulation type reactor, in which at least the circulation type reactor 3 is uniformly heated with a micro wave, a continuous synthesizing device having the circulation type reactors 3 and 10 in pre- and subsequent- stages, a means for uniformly heating at least the circulation type reactor 3 with the micro wave in which the circulation reactor 3 is a reactor for synthesizing a metal core and the circulation type reactor 10 is a reaction tube for synthesizing an oxide shell, and a core shell structure nanoparticle synthesized by the continuous synthesizing method and/or the continuous synthesizing device.;SELECTED DRAWING: Figure 1;COPYRIGHT: (C)2019,JPO&INPIT
机译:解决的问题:提供一种以较少的过程连续合成纳米颗粒而不产生粒径或聚集变化的方法和装置,以及核壳结构纳米颗粒。;解决方案:涉及一种核的连续合成方法。壳结构纳米粒子,其包括:在包括至少一个步骤的循环型反应器的前段中,通过循环型反应器3连续地合成直径为1至100nM的金属纳米粒子,并且在随后的循环型反应器10中水解氧化物前体。 -级,包括至少一个步骤的循环型反应器,其中至少循环型反应器3被微波均匀加热;-连续合成装置,其在前阶段和后阶段具有循环型反应器3和10;用于至少用微波均匀加热循环型反应器3,其中循环反应器3是用于合成金属核,循环型反应器10是用于合成氧化物壳和通过连续合成方法和/或连续合成装置合成的核壳结构纳米粒子的反应管。选图:图1;版权:( C)2019,日本特许厅

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