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Method of obtaining microporous carbon materials enriched with nanoparticles of iron compounds

机译:获得富含铁化合物纳米颗粒的微孔碳材料的方法

摘要

The purpose of the notification is to obtain the carbon materials consisting of the preparation of a solution of water, ethanol, ammonia water, resorcine, potassium oxoate and formalin, the mixing of the solution at room temperature and the treatment of the solution by pressure in a solar thermal microwave reactor for a 15-minute period at pressure. from 1-MPa to 3-MPa, the material obtained is then charred in the argon atmosphere by increasing the temperature by 1-oC/min to 350-oC, holding the material for two hours at this temperature,Thereafter, by increasing the temperature of 1,C/min to the temperature of 600,C-800,C and keeping the sample at the specified temperature for two hours, after which the material is washed with distilled water and dry, it is characterised,that an iron citrate or iron nitrate (III) is added to the solution before formalin is added in such a quantity that the weight of the carbon atoms of the resorcine to the iron atoms of iron citrate or iron nitrate (III) is 10:1.
机译:通报的目的是获得碳材料,该碳材料包括水,乙醇,氨水,间苯二酚,草酸钾和福尔马林溶液的制备,室温下溶液的混合以及压力下的溶液处理。太阳能热微波反应器在压力下持续15分钟。从1-MPa到3-MPa,然后通过以1oC / min的速度将温度升至350oC,在此温度下保持两个小时,然后在温度升高的情况下,在氩气气氛中烧焦以1,C / min的速度加热至600,C-800,C的温度,并将样品在指定温度下保持2小时,然后用蒸馏水洗涤该材料并干燥,其特征是柠檬酸铁或在添加福尔马林之前,将硝酸铁(III)添加到溶液中,其数量应使得间苯二酚的碳原子与柠檬酸铁或硝酸铁(III)的铁原子的重量为10:1。

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