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Fracture toughness of a zirconia engineering ceramic and the effects thereon of surface processing with fibre laser radiation

机译:氧化锆工程陶瓷的断裂韧性及其对纤维激光辐射表面处理的影响

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摘要

Vickers hardness indentation tests were employed to investigate the near-surface changes in the hardness of a fibre laser-treated and an as-received ZrO2 engineering ceramic. Indents were created using 5, 20, and 30 kg loads to obtain the hardness. Optical microscopy, white-light interferometry, and a coordinate measuring machine were then used to observe the crack lengths and crack geometry. Palmqvist and half-penny median crack profiles were found, which dictated the selection of the group of equations used herein. Computational and analytical approaches were then adapted to determine the K1c of ZrO2. It was found that the best applicable equation was: K1c = 0.016 (E/H)1/2 (P/c3/2), which was confirmed to be 42 per cent accurate in producing K1c values within the range of 8 to 12 MPa m1/2 for ZrO2. Fibre laser surface treatment reduced the surface hardness and produced smaller crack lengths in comparison with the as-received surface. The surface crack lengths, hardness, and indentation loads were found to be important, particularly the crack length, which significantly influenced the end K1c value when K1c = 0.016 (E/H)1/2 (P/c3/2) was used. This is because, the longer the crack lengths, the lower the ceramic's resistance to indentation. This, in turn, increased the end K1c value. Also, the hardness influences the K1c, and a softer surface was produced by the fibre laser treatment; this resulted in higher resistance to crack propagation and enhanced the ceramic's K1c. Increasing the indentation load also varied the end K1c value, as higher indentation loads resulted in a bigger diamond footprint, and the ceramic exhibited longer crack lengths.
机译:使用维氏硬度压痕测试来研究经激光处理和原样接收的ZrO2工程陶瓷的硬度在近表面的变化。使用5、20和30 kg的载荷创建压痕以获得硬度。然后使用光学显微镜,白光干涉仪和坐标测量机观察裂纹长度和裂纹几何形状。发现了Palmqvist和半便士的中值裂纹轮廓,这决定了此处使用的方程组的选择。然后采用计算和分析方法确定ZrO2的K1c。已发现最佳适用方程为:K1c = 0.016(E / H)1/2(P / c3 / 2),在产生8至12 MPa范围内的K1c值时,经证实精确度为42%。 ZrO2的m1 / 2。与原样的表面相比,光纤激光表面处理降低了表面硬度并产生了较小的裂纹长度。发现表面裂纹长度,硬度和压痕载荷很重要,特别是裂纹长度,当使用K1c = 0.016(E / H)1/2(P / c3 / 2)时,裂纹长度会显着影响最终K1c值。这是因为裂纹长度越长,陶瓷的抗压痕性越低。这反过来又增加了末端K1c值。而且,硬度会影响K1c,并且通过光纤激光处理会产生更柔软的表面。这导致了更高的抗裂纹扩展能力,并增强了陶瓷的K1c。压痕载荷的增加也改变了最终的K1c值,因为更高的压痕载荷导致了更大的金刚石覆盖区,并且陶瓷表现出了更长的裂纹长度。

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