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Shrinkage stress and elastic modulus assessment of bulk-fill composites

机译:散装复合材料的收缩应力和弹性模量评估

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摘要

Abstract Bulk-fill composites were introduced in dentistry to accelerate clinical procedures while providing adequate outcomes. Concerns regarding the use of bigger composite increments rely on the polymerization shrinkage and shrinkage stress, which may generate gaps on the adhesive interface and result in a reduced success rate. Objective: To evaluate the polymerization shrinkage stress of different bulk-fill resin composites and their elastic modulus. Materials and Methods: Fourteen specimens were made for each of the nine different resin composites (seven with 12 mm3 and seven with 24 mm3): Surefill SDR flow (SDR), X-tra Base (XB), Filtek Bulk Fill Flowable (FBF), Filtek Z350XT Flow (Z3F); Tetric Evo Ceram Bulk Fill (TBF), X-tra Fil (XF), Filtek Bulk Fill (FBP), Admira Xtra Fusion (ADM) and Filtek Z350 XT (Z3XT). Linear shrinkage stress was evaluated for 300 s with the aid of a linear shrinkage device adapted to a Universal Testing Machine. For each composite group, seven additional specimens (2x2x25 mm) were made and Young's modulus was evaluated with a 3-point bending device adapted in a Universal Testing Machine with 0.5 mm/min crosshead speed and 50 KgF loading cell. Results: For 12 mm3 specimens, three-way ANOVA showed that only SDR and TBF generated lower stress after 20 s. Considering 300 s, TBF, SDR, and XF generated the lowest stress, followed by ADM, FBP, XB, and FBF, which were similar to Z3XT. Z3F generated the highest stress values for all time points. Considering 24 mm3 specimens after 20 s, all bulk fill composites generated lower stress than Z3XT, except XB. After 300 s, SDR, FBP, and ADM generated the lowest stress, followed by TBF and XF. For elastic modulus, one-way ANOVA showed that FBF, SDR, Z3F, and ADM presented the lowest values, followed by XB and TBF. FBP, Z3XT, and XF presented the highest elastic modulus among the evaluated composites. Conclusions: Bulk-fill resin composites presented equal to lower shrinkage stress generation when compared to conventional composites, especially when bigger increments were evaluated. Bulk-fill composites showed a wide range of elastic modulus values, but usually similar to “regular” composites.
机译:在牙科介绍了抽象的批量填充复合材料,以加速临床程序,同时提供足够的结果。关于使用更大的复合增量的担忧依赖于聚合收缩和收缩应力,这可能会在粘合剂界面上产生间隙并导致降低的成功率。目的:评价不同堆积树脂复合材料的聚合收缩应力及其弹性模量。材料和方法:为九个不同树脂复合材料中的每一个进行14项样品(具有12mm3和24 mm3的七个):确保SDR流(SDR),X-TRA基础(XB),Filtek散装填充可流动(FBF) ,Filtek Z350xt流(Z3F); Tetric Evo Ceram批量填充(TBF),X-Trafor(XF),Filtek批量填充(FBP),Admira Xtra Fusion(ADM)和Filtek Z350 XT(Z3XT)。借助于适用于通用试验机的线性收缩装置,评估线性收缩应力300秒。对于每个复合材料组,制备七个额外的样品(2x2x25mm),并在具有0.5mm / min的十字头速度和50kgf装载单元的通用试验机中进行三点弯曲装置评价杨氏模量。结果:对于12 mm3标本,三通ANOVA显示,仅在20秒后才能产生低应力。考虑到300秒,TBF,SDR和XF产生最低应力,然后是ADM,FBP,XB和FBF,类似于Z3XT。 Z3F为所有时间点产生最高的应力值。考虑到20秒后的24 mm3标本,除XB之外,所有散装填充复合材料都会产生比Z3x更低的应力。 300秒后,SDR,FBP和ADM产生最低应力,其次是TBF和XF。对于弹性模量,单向ANOVA显示FBF,SDR,Z3F和ADM呈现最低值,其次是XB和TBF。 FBP,Z3XT和XF在评估的复合材料中呈现了最高弹性模量。结论:与常规复合材料相比,批量填充树脂复合材料等于较低的收缩应力产生,特别是当评估更大的增量时。批量填充复合材料显示出广泛的弹性模量值,但通常类似于“常规”复合材料。

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