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A green route to preparation of silica powders with rice husk ash and waste gas

机译:用稻壳灰和废气制备二氧化硅粉的绿色途径

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摘要

The objective of the present work is to develop a green procedure for preparation of silica powders from rice husk ash (RHA) via a carbonation route. The raw materials, RHA and waste gas, were obtained from the power plant. Na2CO3 was used as the silica extraction reagent and waste gas was the precipitator. The silicon dioxide extraction yield reached 72.52% and was affected by impregnation ratio, concentration of Na2CO3 solution and reaction time. The microstructures of the as-obtained silica powders were characterized by X-ray diffraction (XRD) and infrared spectra (1R). The mineral contents of RHA and product were investigated by inductively coupled plasma (ICP) emission spectroscopy. In the whole silica extraction process, extraction reagent can be reused through appended a small quantity of Na2CO3 to its initial concentration. The synthetic procedure is straightforward, inexpensive and environment-friendly, which was suitable for large-scale production.
机译:本工作的目的是开发一种绿色方法,通过碳酸化途径由稻壳灰(RHA)制备二氧化硅粉末。原料,RHA和废气是从电厂获得的。 Na2CO3用作二氧化硅萃取剂,废气为沉淀剂。二氧化硅的提取率达到72.52%,并受浸渍率,Na2CO3溶液浓度和反应时间的影响。通过X射线衍射(XRD)和红外光谱(1R)表征所获得的二氧化硅粉末的微观结构。 RHA和产品的矿物质含量通过电感耦合等离子体(ICP)发射光谱法进行了研究。在整个二氧化硅萃取过程中,可以通过向其初始浓度中添加少量的Na2CO3来重复使用萃取剂。该合成方法简单,便宜且对环境友好,适合大规模生产。

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