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Optical studies of nano-structured La-doped ZnO prepared by combustion method

机译:燃烧法制备纳米结构掺镧ZnO的光学研究

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摘要

Coral-shaped nano-structured zinc oxide (ZnO) was successfully synthesized and La-doped via a facile combustion process using glycine as a fuel. The auto-ignition (at -185 ℃) of viscous reactants zinc nitrate and glycine resulted in ZnO powders. Hexagonal wurtzite structure of pure and doped ZnO powder was confirmed by X-ray powder diffraction analysis. The transmission electron micrograph shows that the nano-structured ZnO is coral-shaped and possess maximal pore ( —10-50 nm pore size) density in it and the grain size is approximately about 15 nm. Addition of dopants subsequently alters the structural and optical properties which were confirmed by UV-VIS studies.
机译:成功地合成了珊瑚状的纳米结构的氧化锌(ZnO),并使用甘氨酸作为燃料通过易燃的燃烧过程进行了La掺杂。粘性反应物硝酸锌和甘氨酸的自燃(在-185℃下)产生ZnO粉。 X射线粉末衍射分析证实了纯净掺杂ZnO粉末的六方纤锌矿结构。透射电子显微照片显示,纳米结构的ZnO是珊瑚形的,并且具有最大的孔(孔径为-10-50 nm),并且晶粒尺寸约为15 nm。掺杂剂的添加随后改变了结构和光学性质,这通过UV-VIS研究得到证实。

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