Microstructural, mechanical and electrochemical characterisation of biomaterial ASTM F745 cast by vacuum

摘要

Countergravity low pressure casting (CLA) was performed to enhance the properties of ASTM F745 stainless steel (SS), which is usually used as biomaterial. The macro- and microstructures were compared with those obtained by the conventional process of investment casting (IC). The SS cast by CLA (SSCLA) exhibited a smaller size of solidification cell and finer dendritic microstructure. The average of its dendritic primary spacing was 110.4 μm, while for the same steel cast by IC (SSIC), it was 186.7 μm. The density of non-metallic inclusions δ_1 in the SSCLA was 717 I mm~(-2), being the majority of them smaller than 1.5 μm. In the case of SSIC, δ_1 was852 I mm~(-2), with a size distribution of up to 8 μm. The SSCLA showed a higher breakdown potential than the SSIC, the values being 0.300 and 0.210 V(saturated calomel electrode) respectively, which means a higher resistance to suffer localised corrosion. Finely, the CLA process also allowed obtaining better mechanical properties.