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Crystal defects in dense hydrous magnesium silicate phase A deformed at high pressure: characterization by transmission electron microscopy

机译:高压变形的致密含水硅酸镁A相中的晶体缺陷:通过透射电子显微镜表征

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摘要

Dense hydrous magnesium silicate (DHMS) Phase A has been deformed at 11 GPa, 700 and 400 °C in the multianvil apparatus. Transmission electron microscopy (TEM) characterizations, using the weak-beam dark-field (WBDF) technique, have shown that at 700 °C, two different types of perfect dislocations are activated with 1/3?2īī0? and 1/3 ?2īī3?; Burgers vectors. The 1/3?2īī0?dislocations glide in the basal plane, but for 1/3?2īī3? dislocations, no glide plane could be identified. At 400 °C, dissociation of 1/3?2īī0?dislocations is observed in the basal plane. Furthermore, prismatic and pyramidal glide planes were identified, with dissociations in pyramidal planes, at this temperature. Also a growth reticular merohedral twin has been observed; the twin law results from a rotation of 180° around the [1540] axis.
机译:在多砧装置中,致密含水硅酸镁(DHMS)A在11 GPa,700和400°C下变形。使用弱束暗场(WBDF)技术的透射电子显微镜(TEM)表征表明,在700°C时,两种不同类型的完美位错被1/3?2?0激活。和1/3?2īī3?;汉堡向量。 1/3?2?0?位错在基面上滑动,但1/3?2?3?位错。脱位,无法确定滑行平面。在400°C,在基面上观察到1/3?2?0?位错的解离。此外,在此温度下,确定了棱柱形和金字塔形滑行平面,并且在金字塔形平面中有解离。还观察到了生长网状双面体双胞胎。孪生定律是绕[1540]轴旋转180°的结果。

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