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Fabrication and characterization of optical-fiber nanoprobes for scanning near-field optical microscopy

机译:扫描近场光学显微镜用光纤纳米探针的制备与表征

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The current scanning near-field optical microscopy has been developed with optical-fiber probes obtained by use of either laser-heated pulling or chemical etching. For high-resolution near-field imaging, the detected signal is rapidly attenuated as the aperture size of the probe decreases. It is thus important to fabricate probes optimized for both spot size and optical transmission. We present a two-step fabrication that allowed us to achieve an improved performance of the optical-fiber probes. Initially, a CO2 laser-heated pulling was used to produce a parabolic transitional taper ending with a top thin filament. Then, a rapid chemical etching with 50% buffered hydrofluoric acid was used to remove the thin filament and to result in a final conical tip on the top of the parabolic transitional taper. Systematically, we obtained optical-fiber nanoprobes with the apex size as small as 10 nm and the final cone angle varying from 15 degrees to 80 degrees. It was found that the optical transmission efficiency increases rapidly as the taper angle increases from 15 degrees to 50 degrees, but a further increase in the taper angle gives rise to important broadening of the spot size. Finally, the fabricated nanoprobes were used in photon-scanning tunneling microscopy, which allowed observation of etched double lines and grating structures with periods as small as 200 nm. (C) 1998 Optical Society of America. [References: 29]
机译:当前的扫描近场光学显微镜已经开发了使用通过激光加热拉动或化学蚀刻获得的光纤探针。对于高分辨率近场成像,随着探头孔径的减小,检测到的信号会迅速衰减。因此,重要的是制造针对光点尺寸和光传输均经过优化的探头。我们提出了两步制造法,使我们能够提高光纤探针的性能。最初,使用CO2激光加热拉制产生抛物线过渡的锥度,并以顶部细丝结束。然后,用50%的氢氟酸缓冲液进行快速化学蚀刻,以去除细丝,并在抛物线过渡锥的顶部形成最终的锥形尖端。系统地,我们获得了顶点尺寸小至10 nm,最终锥角从15度到80度变化的光纤纳米探针。已经发现,随着锥角从15度增加到50度,光传输效率迅速增加,但是锥角的进一步增加引起光斑尺寸的重要加宽。最后,将制成的纳米探针用于光子扫描隧道显微镜,可以观察到蚀刻的双线和周期短至200 nm的光栅结构。 (C)1998年美国眼镜学会。 [参考:29]

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