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首页> 外文期刊>Analytical Biochemistry: An International Journal of Analytical and Preparative Methods >A low volume 3D-printed temperature-controllable cuvette for UV visible spectroscopy
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A low volume 3D-printed temperature-controllable cuvette for UV visible spectroscopy

机译:用于紫外可见光谱的小体积3D打印温度控制比色皿

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摘要

We report the fabrication of a 3D-printed water-heated cuvette that fits into a standard UV visible spectrophotometer. Full 3D-printable designs are provided and 3D-printing conditions have been optimised to provide options to print the cuvette in either acrylonitrile butadiene styrene or polylactic acid polymers, extending the range of solvents that are compatible with the design. We demonstrate the efficacy of the cuvette by determining the critical micelle concentration of sodium dodecyl sulphate at 40 degrees C, the molar extinction coefficients of cobalt nitrate and dsDNA and by reproducing the thermochromic UV visible spectrum of a mixture of cobalt chloride, water and propan-2-ol. (C) 2016 Elsevier Inc. All rights reserved.
机译:我们报告了3D打印水加热比色皿的制造过程,该比色皿适合标准的UV可见分光光度计。提供了完整的3D可打印设计,并优化了3D打印条件,以提供在丙烯腈丁二烯苯乙烯或聚乳酸聚合物中打印比色杯的选项,从而扩展了与该设计兼容的溶剂范围。我们通过确定40°C时十二烷基硫酸钠的临界胶束浓度,硝酸钴和dsDNA的摩尔消光系数,以及通过再现氯化钴,水和丙烷的混合物的热致变色紫外可见光谱,来证明比色皿的功效。 2-醇。 (C)2016 Elsevier Inc.保留所有权利。

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