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3D Printed UV–Visible Cuvette Adapter for Low-Costand Versatile Spectroscopic Experiments

机译:3D打印的紫外线​​可见比色皿适配器可实现低成本和多功能光谱实验

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摘要

Ultraviolet–visible (UV–vis) spectroscopy represents one of the most popular analytical techniques in chemical research labs. A variety of vendors provide instruments that are suited for the analysis of liquid samples at moderate concentrations. However, to accommodate more specialized experiments, expensive accessories are required and often do not fit the specific needs of experimental scientists. In this work, we present a generalized adapter that can be 3D printed and used with existing spectrometers to enable a wide array of experiments to be performed. In the case of liquid samples, we provide a method for dramatically reducing the price of a quartz cuvette with minimal impact on performance. Through simple modification of the design, cuvettes with various path lengths can be prepared. Additionally, we illustrate the ability to turn any sample container into a working cuvette to simplify experimental protocols, prevent contamination risks, and further reduce costs. This strategy also enables gaseous and solid samples to be evaluated easily and reproducibly.Furthermore, we demonstrate how this concept can be extended to interfaceadditional instrumentation with a commercial UV–vis spectrometer.All of the digital designs are provided under a creative commons licenseto enable other researchers to modify and adapt the designs for theirunique experimental requirements.
机译:紫外可见光谱是化学研究实验室中最流行的分析技术之一。许多供应商提供了适合于中等浓度液体样品分析的仪器。但是,为了适应更专业的实验,需要昂贵的附件,并且通常不符合实验科学家的特定需求。在这项工作中,我们介绍了一种通用适配器,该适配器可以进行3D打印并与现有的光谱仪配合使用,以进行各种各样的实验。对于液体样品,我们提供了一种在不影响性能的情况下大幅降低石英比色皿价格的方法。通过简单的设计修改,可以制备出具有各种光程长度的比色皿。此外,我们展示了将任何样品容器变成工作比色皿的能力,以简化实验方案,防止污染风险并进一步降低成本。这种策略还可以轻松,可重复地评估气态和固态样品。此外,我们演示了如何将该概念扩展到接口带有商用紫外可见光谱仪的其他仪器。所有数字设计均在知识共享许可下提供使其他研究人员可以针对他们的设计进行修改和调整独特的实验要求。

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