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首页> 外文期刊>Current Analytical Chemistry >Real Time Detection of Aroma Compounds in Meat and Meat Products by SIFT-MS and Comparison to Conventional Techniques (SPME-GC-MS)
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Real Time Detection of Aroma Compounds in Meat and Meat Products by SIFT-MS and Comparison to Conventional Techniques (SPME-GC-MS)

机译:通过SIFT-MS实时检测肉类和肉类产品中的香气化合物,并与常规技术进行比较(SPME-GC-MS)

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摘要

The applicability of selected ion flow tube mass spectrometry, SIFT-MS, for the study of the quality of meat and meat products in comparison to conventional techniques (SPME-GC-MS) has been investigated. To this end, two different approaches were followed. The first was to study the release of aroma compounds after saliva addition to fermented sausages and the second, the application of SIFT-MS and SPME-GC-MS to the detection of chemical spoilage in retail meat (raw and cooked). The headspace (HS) concentration of volatile compounds was influenced by saliva addition to the fermented sausage. SIFT-MS obtained better correlations than SPME-GC-MS between compound release and their molecular weight, MW, and hydrophobicity properties. Saliva differentially affected the release of the compounds, suppressing the release of hydrophilic and low MW compounds and either having little effect or enhancing the release of hydrophobic and higher MW compounds. These results provide preliminary explanations of aroma perception during eating. In addition, SIFT-MS was able to detect differences in the same way as SPME-GC-MS in fresh beef meat during refrigerated storage, but the differences were hardly detectable in cooked meat. Therefore, SIFT-MS can be used as a fast monitor of lipid oxidation changes in retail meat packaged in high oxygen atmospheres.
机译:与常规技术(SPME-GC-MS)相比,已研究了所选离子流管质谱仪SIFT-MS在研究肉类和肉制品质量方面的适用性。为此,采用了两种不同的方法。首先是研究唾液添加到发酵香肠中后释放的香气化合物,其次是将SIFT-MS和SPME-GC-MS用于检测零售肉(生肉和熟肉)中的化学变质情况。挥发性化合物的顶空(HS)浓度受发酵香肠中唾液添加的影响。 SIFT-MS在化合物释放与其分子量,分子量和疏水性之间比SPME-GC-MS具有更好的相关性。唾液差异地影响了化合物的释放,抑制了亲水性和低分子量化合物的释放,效果不佳或增强了疏水性和较高分子量化合物的释放。这些结果提供了进食期间对香气感知的初步解释。此外,SIFT-MS能够以与SPME-GC-MS相同的方式在冷藏过程中检测鲜牛肉中的差异,但在熟肉中几乎检测不到差异。因此,SIFT-MS可以用作在高氧气氛下包装的零售肉类中脂质氧化变化的快速监控器。

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