PASE synthesis of 1-azolyl-1H-1,2,4-triazoles by the reaction of diazoazoles with ethyl isocyanoacetate

Sadchikova Elena V; Alexeeva Daria L.; Nenajdenko Valentine G.

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PASE synthesis of 1-azolyl-1H-1,2,4-triazoles by the reaction of diazoazoles with ethyl isocyanoacetate

机译：用二唑唑与异氰酸乙酯反应的1-唑唑-1H-1,2,4-三唑的合成

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摘要

PASE (pot, atom and step economic) synthesis of 1-azolyl-1H-1,2,4-triazole derivatives in up to 91% yield has been accomplished by addition of 5-diazoazoles to ethyl isocyanoacetate.

机译：通过向异氰酸乙酸乙酯加入5-二唑唑来实现1-唑醇-1H-1,2,4-三唑衍生物的1-唑酯-1H-1,2,4-三唑衍生物的合成，得到了高达91％的产率。

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《Mendeleev Communications 》 |2019年第6期| 共2页
作者
Sadchikova Elena V; Alexeeva Daria L.; Nenajdenko Valentine G.;
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Ural Fed Univ Inst Chem Engn Ekaterinburg 620002 Russia;

Ural Fed Univ Inst Chem Engn Ekaterinburg 620002 Russia;

Moscow MV Lomonosov State Univ Dept Chem Moscow 119991 Russia;

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中图分类化学 ;
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1. PASE synthesis of 1-azolyl-1H-1,2,4-triazoles by the reaction of diazoazoles with ethyl isocyanoacetate [J] . Sadchikova Elena V, Alexeeva Daria L., Nenajdenko Valentine G. Mendeleev Communications . 2019 ,第6期

机译：用二唑唑与异氰酸乙酯反应的1-唑唑-1H-1,2,4-三唑的合成
2. Reactions of P-alkoxyvinyl polyfluoroalkyl ketones with ethyl isocyanoacetate and its use for the synthesis of new polyfluoroalkyl pyrroles and pyrrolidines [J] . Ivan S. Kondratov, Violetta G. Dolovanyuk, Nataliya A. Tolmachova, Organic & biomolecular chemistry . 2012 ,第44期

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3. Synthesis of bis-armed amino acid derivatives via the alkylation of ethyl isocyanoacetate and the Suzuki-Miyaura cross-coupling reaction [J] . S.Kotha, V.R.Shah, S.Haider Amino acids . 2007 ,第3期

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4. Synthesis of Organotin Polyamines from Reaction of 3-Amino-1,2,4-triazole and Organotin Dihalides [C] . Charles E. Carraher Jr., Ryan Crichton, Michael R. Roner American Chemical Society Division of Polymeric Materials Science and Engineering Conference . 2015

机译：3-氨基-1,2,4-三唑和有机锡二卤化物反应的有机素多胺的合成
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6. Direct Catalytic Enantio- and Diastereoselective Ketone Aldol Reactions of Isocyanoacetates [O] . Dr. Raquel delaCampa, Dr. Irene Ortín, Prof.Dr. Darren J Dixon -1

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7. Flow synthesis of ethyl isocyanoacetate enabling the telescoped synthesis of 1,2,4-triazoles and pyrrolo-1,2-cpyrimidines. [O] . Baumann M., Rodriguez Garcia A. M., Baxendale I. R. 2015

机译：异氰基乙酸乙酯的流式合成能够实现1,2,4-三唑和吡咯并-1,2-c嘧啶的伸缩合成。

PASE synthesis of 1-azolyl-1H-1,2,4-triazoles by the reaction of diazoazoles with ethyl isocyanoacetate

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