A Zirconium Oxide Nanoparticle Modified Screen‐printed Electrode for Anodic Stripping Determination of Daclatasvir Dihydrochloride

Hendawy Hassan A. M.; Eldin Ghada M. G.; Fekry Amany M.

摘要

Abstract > A novel, sensitive and rapid voltammetric method applied for daclatasvir dihydrochloride (DSV.2HCl) detection in raw material, human plasma and urine using square wave voltammetry at a nano‐screen printed electrode (SPE) based on synthesized zirconium oxide nanoparticles (ZrO <sub>2</sub> NPs). The attention to zirconium oxide nanoparticle syntheses arises from its likely use in making an electrode material in the electroanalytical process. Anodic stripping square wave voltammetric peaks have been recorded at the optimum conditions of drug solution as pH, scan rate, accumulation time and accumulation potential. Morphology of the used nanoparticles has been performed by scanning electron microscope (SEM) and transmission microscope (TEM). ZrO <sub>2</sub> NPs were applied to screen printed electrode (ZrO <sub>2</sub> ‐MSPE) giving a new sensor to detect the DSV.2HCl drug. ZrO <sub>2</sub> NPs were tested for their electroactivity in improving electrodes sensitivity. The modified electrode has been used for the analysis of DSV.2HCl in spiked serum, spiked urine and pharmaceutical formulation. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</标题> >应用于Daclatasvir二盐酸盐（DSV.2HCL）检测的新型，敏感和快速的伏安法基于合成的氧化锆纳米颗粒（ZrO <Sub> 2 </ Sub> NPS）的纳米丝网印刷电极（SPE）在纳米丝网印刷电极（SPE）处的原料，人血浆和尿液使用方波伏安法。引起氧化锆纳米颗粒合成的注意力从其可能在电扫描过程中制作电极材料的可能性。作为pH，扫描速率，累积时间和累积电位，已经在药物溶液的最佳条件下记录了阳极剥离方波伏安峰。通过扫描电子显微镜（SEM）和透射显微镜（TEM）进行了使用的纳米颗粒的形态。 ZrO <sub> 2 </ sub> nps被施加到筛选印刷电极（ZrO <sub> 2 </ sub> -mspe）上，为新的传感器检测DSV.2HCL药物。测试ZrO <Sub> 2 </ sub> NPS以改善电极灵敏度的电分子。改性电极已用于分析尖刺血清，尖刺尿液和药物制剂中的DSV.2HCL。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2019年第5期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hendawy Hassan A. M.&option=202" target="_blank" rel="nofollow">Hendawy Hassan A. M.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Eldin Ghada M. G.&option=202" target="_blank" rel="nofollow">Eldin Ghada M. G.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fekry Amany M.&option=202" target="_blank" rel="nofollow">Fekry Amany M.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>National Organization for Drug Control and Research (NODCAR)P. O. Box 29 Cairo Egypt;</p> <p>National Organization for Drug Control and Research (NODCAR)P. O. Box 29 Cairo Egypt;</p> <p>Chemistry DepartmentFaculty of Science Cairo UniversityGiza- 12613 Egypt;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Daclatasvir dihydrochloride&option=203" rel="nofollow">Daclatasvir dihydrochloride;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=zirconium oxide&option=203" rel="nofollow">zirconium oxide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=transmission electron microscope&option=203" rel="nofollow">transmission electron microscope;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=scanning electron microscope&option=203" rel="nofollow">scanning electron microscope;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=screen-printed electrode&option=203" rel="nofollow">screen-printed electrode;</a> </p> <div class="translation"> 机译：daclatasvir二盐酸盐;氧化锆;透射电子显微镜;扫描电子显微镜;丝网印刷电极; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704023174284.html">A Zirconium Oxide Nanoparticle Modified Screen‐printed Electrode for Anodic Stripping Determination of Daclatasvir Dihydrochloride</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hendawy Hassan A. 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