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Synthesis and structural properties of ZnO doped nanoparticles prepared by hydrothermal method

机译:水热法制备ZnO掺杂纳米粒子的合成与结构性能

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摘要

The present study investigates the structural properties of pure and doped ZnO nanosized particles. The nanosized particleswere synthesized by using hydrothermal process at room temperature. Nanoparticles have been characterized for its optical, structural properties using UV-VIS spectrophotometer and X-ray diffraction (XRD). XRD results show that the prepared samples have single phase and has hexagonal wurtzite structure. Further, the crystal-lite size of the ZnO nanoparticles have been determined using Scherrer, Williamson Hall method and size strain plot. The different chemical nature and different ionic radii are main effect, which shows different properties for the different dopant as compared to the host cation. Due to the different doping content, the crystallite size of nanoparticles found to be increased. The physical parameters such as strain-stress curve and energy values were calculated for all the reflected peaks of XRD data.
机译:本研究研究了纯净ZnO纳米型颗粒的结构性。 通过在室温下使用水热过程合成纳米化颗粒。 已经使用UV-VIS分光光度计和X射线衍射(XRD)对其进行了光学,结构性能的纳米颗粒。 XRD结果表明,制备的样品具有单相,具有六边形紫硝基钛矿结构。 此外,使用Scherrer,Williamson Hall方法和尺寸应变图确定了ZnO纳米颗粒的晶体含量尺寸。 不同的化学性质和不同的离子半径是主要效果,与宿主阳离子相比,不同掺杂剂的不同性质显示出不同的掺杂剂。 由于掺杂含量不同,发现纳米颗粒的微晶尺寸增加。 计算诸如应变应力曲线和能量值的物理参数,用于XRD数据的所有反射峰。

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