Electrochemically Reduced Graphene Oxide‐Sheltered ZnO Nanostructures Showing Enhanced Electrochemical Performance Revealed by an In Situ Electrogravimetric Study

Gao Wanli; Demir‐Cakan Rezan; Perrot Hubert; Sel Ozlem

摘要

Abstract > The present work is on the synthesis and characterization of vertically aligned ZnO nanostructures sheltered by electrochemically reduced graphene oxide (ERGO), i.e., ZnO@ERGO, which are directly generated on quartz resonators of microbalance sensors. The vertical orientation of the ZnO nanorods is achieved by a two‐step synthesis method involving an electrochemically grown seed layer and a subsequent hydrothermal growth. Deposited ERGO thin layer turns out to be highly effective to enhance the electrochemical performances of vertically oriented ZnO nanorods as supercapacitor electrodes. The interfacial charge storage mechanism of ZnO@ERGO electrodes with unique architecture is first studied by classical electrochemical quartz crystal microbalance (EQCM), showing a global cation‐exchange behavior in Na <sub>2</sub> SO <sub>4</sub> electrolyte. A complementary technique, electrogravimetric impedance spectroscopy, is then used to deconvolute the EQCM response into individual contributions from Na + ·H <sub>2</sub> O, SO <sub>4</sub> 2? , and H <sub>2</sub> O molecules, offering a quantitative picture of each participant in the charge balance process with their transfer kinetics. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 本作本作通过电化学减少的石墨烯氧化物（ERGO），即ZnO @ Ergo施舍的垂直对准ZnO纳米结构的合成和表征，直接在微稳态传感器的石英谐振器上直接产生。通过涉及电化学生长的种子层和随后的水热生长的两步合成方法实现ZnO纳米棒的垂直取向。沉积的ERGO薄层透明于高效，以提高垂直定向的ZnO纳米棒作为超级电容器电极的电化学性能。首先通过经典电化学石英晶体微稳定（EQCM）研究具有独特架构的ZnO @ ergo电极的界面电荷存储机制，显示了NA中的全球阳离子交换行为 <sub> 2 </ sub> 所以 <sub> 4 </ sub> 电解质。互补技术，电解阻抗光谱，然后用于将EQCM响应解构到NA的个体贡献中 + </ sup> ·H <sub> 2 </ sub> o，所以 <sub> 4 </ sub> 2？</ sup> 和h. <sub> 2 </ sub> o分子，为每位参与者提供定量图片，以其转移动力学。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2019年第5期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gao Wanli&option=202" target="_blank" rel="nofollow">Gao Wanli;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Demir‐Cakan Rezan&option=202" target="_blank" rel="nofollow">Demir‐Cakan Rezan;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Perrot Hubert&option=202" target="_blank" rel="nofollow">Perrot Hubert;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sel Ozlem&option=202" target="_blank" rel="nofollow">Sel Ozlem;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Sorbonne UniversitéLISEF‐75005 Paris France;</p> <p>Department of Chemical EngineeringGebze Techical University41400 Gebze Kocaeli Turkey;</p> <p>Sorbonne UniversitéLISEF‐75005 Paris France;</p> <p>Sorbonne UniversitéLISEF‐75005 Paris France;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrogravimetry&option=203" rel="nofollow">electrogravimetry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrochemical quartz crystal microbalance&option=203" rel="nofollow">electrochemical quartz crystal microbalance;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=interfacial ion transfer&option=203" rel="nofollow">interfacial ion transfer;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanostructured electrodes&option=203" rel="nofollow">nanostructured electrodes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=supercapacitors&option=203" rel="nofollow">supercapacitors;</a> </p> <div class="translation"> 机译：电化学杂志;电化学石英晶体微稳定;界面离子转移;纳米结构电极;超级电容器; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022435555.html">Electrochemically Reduced Graphene Oxide‐Sheltered ZnO Nanostructures Showing Enhanced Electrochemical Performance Revealed by an In Situ Electrogravimetric Study</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gao Wanli&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Gao Wanli,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Demir‐Cakan Rezan&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Demir‐Cakan Rezan,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Perrot Hubert&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Perrot Hubert,</a> <a href="/journal-foreign-18063/" target="_blank" rel="nofollow" class="tuijian_authcolor">Advanced materials interfaces .</a> <span>2019</span><span>,第5期</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：电化学还原的石墨烯氧化物避难ZnO纳米结构，显示出通过原位电解研究显示的增强电化学性能</span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-journal-foreign_applied-surface-science_thesis/0204111667697.html">Enhanced photocatalytic performance of ZnO nanostructures by electrochemical hybridization with graphene oxide</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pruna A.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Pruna A.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wu Z.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Wu Z.,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zapien J. 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