Enhanced NO        <i >          <sub>x</sub>                  <sub >x</sub>x                Gas Sensing Properties of Ordered Mesoporous WO        <sub >3</sub>3        /ZnO Prepared by Electroless Plating

Han Ji; Wang Tian‐yang; Li Tian‐tian; Yu Hui; Yang Ying; Dong Xiang‐ting

摘要

Abstract > A kind of novel n–n combined ordered mesoporous WO <sub>3</sub> /ZnO (OM‐WO <sub>3</sub> /ZnO) sensor are successfully fabricated in this study. A soft‐template method is used to synthesize the ordered mesoporous ZnO matrix. Surfaces of the ZnO matrix are innovatively modified using silane coupling agent (mark as: OM‐ZnO‐Si), and then a layer of WO <sub>3</sub> film is assembled on the surfaces of the OM‐ZnO‐Si by chemical plating method for the first time, and the OM‐WO <sub>3</sub> /ZnO material is obtained. The prepared OM‐WO <sub>3</sub> /ZnO sample shows a kind of regular hexagon‐sheet structure. The prepared OM‐WO <sub>3</sub> /ZnO sensor shows the much better response, much shorter response time, much lower detection limit, and the more excellent selectivity toward NO <sub>x</sub> gas. When oxynitride (NO <sub>x</sub> ) gas concentration is 100 ppm, the response reaches to 82.64%, the response time is only 6 s at room temperature. The detection limit is only 0.01 ppm. The unique loose porous structure and the synergistic effect of the n–n heterojunction structure endow the prepared OM‐WO <sub>3</sub> /ZnO material with the superior gas sensing properties. The n–n combined OM‐WO <sub>3</sub> /ZnO material shows the vast development potential in gas sensor field. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 一种新的n-n组合有序的介孔wo <sub> 3 </ sub> / zno（om-wo <sub> 3 </ sub> / ZnO）传感器在本研究中成功制造。软模板方法用于合成有序的中孔ZnO矩阵。 ZnO矩阵的表面采用硅烷偶联剂（标记为：OM-ZnO-Si）创新地修饰，然后是一层WO <sub> 3 </ sub> 首次通过化学电镀方法在OM-ZnO-Si的表面上组装薄膜，以及OM-WO <sub> 3 </ sub> / ZnO材料获得。准备好的om-wo <sub> 3 </ sub> / ZnO样品显示了一种常规六边形板结构。准备好的om-wo <sub> 3 </ sub> / ZnO传感器显示了更好的反应，响应时间更短，检测极限更低，以及对NO更出色的选择性 <sub> x </ sub> </ i> 气体。氧氮化物（没有 <sub> x </ sub> </ i> ）气体浓度为100ppm，响应达到82.64％，响应时间在室温下仅6秒。检测限仅为0.01ppm。独特的松散多孔结构和N-N异质结构的协同效果赋予制备的OM-WO <sub> 3 </ sub> / ZnO材料具有优异的气体传感性能。 n-n组合om-wo <sub> 3 </ sub> / ZnO材料显示了气体传感器领域的广阔发展潜力。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-18063/'>《Advanced materials interfaces》</a> <b style="margin: 0 2px;">|</b><span>2018年第9期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Han Ji&option=202" target="_blank" rel="nofollow">Han Ji;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Tian‐yang&option=202" target="_blank" rel="nofollow">Wang Tian‐yang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Tian‐tian&option=202" target="_blank" rel="nofollow">Li Tian‐tian;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yu Hui&option=202" target="_blank" rel="nofollow">Yu Hui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Ying&option=202" target="_blank" rel="nofollow">Yang Ying;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Dong Xiang‐ting&option=202" target="_blank" rel="nofollow">Dong Xiang‐ting;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of Chemistry and Environmental EngineeringChangchun University of Science and TechnologyChangchun 130022 P. R. China;</p> <p>School of Chemistry and Environmental EngineeringChangchun University of Science and TechnologyChangchun 130022 P. R. China;</p> <p>School of Chemistry and Environmental EngineeringChangchun University of Science and TechnologyChangchun 130022 P. R. China;</p> <p>School of Chemistry and Environmental EngineeringChangchun University of Science and TechnologyChangchun 130022 P. R. China;</p> <p>School of Chemistry and Environmental EngineeringChangchun University of Science and TechnologyChangchun 130022 P. R. China;</p> <p>School of Chemistry and Environmental EngineeringChangchun University of Science and TechnologyChangchun 130022 P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/6960.html" title="特种结构材料">特种结构材料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electroless plating method&option=203" rel="nofollow">electroless plating method;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=gas sensitivity&option=203" rel="nofollow">gas sensitivity;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=n–n heterojunctions&option=203" rel="nofollow">n–n heterojunctions;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=NO x&option=203" rel="nofollow">NO x;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ordered mesoporous WO 3 /ZnO&option=203" rel="nofollow">ordered mesoporous WO 3 /ZnO;</a> </p> <div class="translation"> 机译：化学镀方法;气体敏感性;n-n异性结;no x;有序的介孔wo 3 / zno; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022434557.html">Electroless Plating Method: Enhanced NO <i > <sub>x</sub> <sub >x</sub>x Gas Sensing Properties of Ordered Mesoporous WO <sub >3</sub>3 /ZnO Prepared by Electroless Plating (Adv. 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2011-10-17</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：化学镀镍溶液，使用其的化学镀方法以及由镍镀层制备的镍镀层 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130424649645.html">NICKEL-PHOSPHORUS-TUNGSTEN ALLOY ELECTROLESS PLATING SOLUTION, AN ELECTROLESS PLATING PROCESS USING THE SAME, AND A NICKEL-PHOSPHORUS-TUNGSTEN ALLOY PLATING LAYER PREPARED BY THE PROCESS</a> <b>[P]</b> . <span> 外国专利：  KR20100120444A </span> <span> . 2010-11-16</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：镍-磷-钨合金化学镀溶液，使用相同的化学镀过程以及由该方法制备的镍-磷-钨合金镀层 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130424430286.html">METHOD FOR ENHANCING FIELD EMISSION PROPERTY OF ZnO NANOWIRES AND METHOD FOR 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Enhanced NO x xx Gas Sensing Properties of Ordered Mesoporous WO 33 /ZnO Prepared by Electroless Plating

摘要

Enhanced NO _x _xx Gas Sensing Properties of Ordered Mesoporous WO ₃3 /ZnO Prepared by Electroless Plating